Technology Process of [Pt(2-(2'-pyridyl)-3,5,6,8-tetramethyl-1,10-phenanthroline)Cl](tetrakis[3,5-bis(trifluoromethyl)phenyl]borate)
There total 1 articles about [Pt(2-(2'-pyridyl)-3,5,6,8-tetramethyl-1,10-phenanthroline)Cl](tetrakis[3,5-bis(trifluoromethyl)phenyl]borate) which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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With
2-(N-morpholine)ethanesulfonic acid; NaCl;
In
water; acetone;
ligandin acetone was added to suspn. Pt(COD)Cl2 in aq. 2-(N-morpholine)ethanesulfonic acid and heated, aq. NaCl was added, ppt. was heated in CH2Cl2 containing Na(BAr4); soln. was filtered, solvent was evapd., residue was recrystd. from CH2Cl2/hexane 1:1; elem. anal.;
DOI:10.1021/ic025922c