Technology Process of C16H19N3
There total 3 articles about C16H19N3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
palladium 10% on activated carbon; hydrogen;
In
ethyl acetate;
under 760.051 Torr;
DOI:10.1016/j.bmcl.2012.11.086
- Guidance literature:
-
Multi-step reaction with 5 steps
1: palladium diacetate; sodium acetate / N,N-dimethyl-formamide / 100 °C
2: trifluoroacetic acid / dichloromethane
3: ethanol / 4 h / 160 °C / Microwave irradiation
4: formic acid / 1,2-dichloro-ethane / 70 °C
5: palladium 10% on activated carbon; hydrogen / ethyl acetate / 760.05 Torr
With
formic acid; palladium 10% on activated carbon; hydrogen; sodium acetate; palladium diacetate; trifluoroacetic acid;
In
ethanol; dichloromethane; ethyl acetate; 1,2-dichloro-ethane; N,N-dimethyl-formamide;
1: |Heck Reaction;
DOI:10.1016/j.bmcl.2012.11.086
- Guidance literature:
-
Multi-step reaction with 5 steps
1: palladium diacetate; sodium acetate / N,N-dimethyl-formamide / 100 °C
2: trifluoroacetic acid / dichloromethane
3: ethanol / 4 h / 160 °C / Microwave irradiation
4: formic acid / 1,2-dichloro-ethane / 70 °C
5: palladium 10% on activated carbon; hydrogen / ethyl acetate / 760.05 Torr
With
formic acid; palladium 10% on activated carbon; hydrogen; sodium acetate; palladium diacetate; trifluoroacetic acid;
In
ethanol; dichloromethane; ethyl acetate; 1,2-dichloro-ethane; N,N-dimethyl-formamide;
1: |Heck Reaction;
DOI:10.1016/j.bmcl.2012.11.086
