C₁₅H₁₄N₂O₃

Base Information

Chemical Name:C₁₅H₁₄N₂O₃
CAS No.:1428147-70-9
Molecular Formula:C₁₅H₁₄N₂O₃
Molecular Weight:270.288
Hs Code.:

C<sub>15</sub>H<sub>14</sub>N<sub>2</sub>O<sub>3</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₅H₁₄N₂O₃

Chemical Property:

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Technology Process of C₁₅H₁₄N₂O₃

There total 3 articles about C₁₅H₁₄N₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 15.0%

: 7021-46-7
5-aminotropolone

: 3173-56-6
benzyl isothiocyanate

: 1428147-70-9
C₁₅H₁₄N₂O₃

Guidance literature:: In tetrahydrofuran; at 95 ℃; for 2h; under 12929 Torr; Microwave irradiation;
DOI:10.1039/c3cc41191e

Reference yield:

: 533-75-5
2-hydroxy-2,4,6-cycloheptatrien-1-one

: 1428147-70-9
C₁₅H₁₄N₂O₃

Guidance literature:: Multi-step reaction with 3 steps

1: acetic acid; sodium nitrite / water / 3 h / 25 °C / Inert atmosphere

2: hydrogen; palladium 10% on activated carbon / ethanol / 18 h / 1137.76 Torr

3: tetrahydrofuran / 2 h / 95 °C / 12929 Torr / Microwave irradiation

With palladium 10% on activated carbon; hydrogen; acetic acid; sodium nitrite; In tetrahydrofuran; ethanol; water;
DOI:10.1039/c3cc41191e

Reference yield:

: 2297-94-1
5-nitrosotropolone

: 1428147-70-9
C₁₅H₁₄N₂O₃

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen; palladium 10% on activated carbon / ethanol / 18 h / 1137.76 Torr

2: tetrahydrofuran / 2 h / 95 °C / 12929 Torr / Microwave irradiation

With palladium 10% on activated carbon; hydrogen; In tetrahydrofuran; ethanol;
DOI:10.1039/c3cc41191e