7-Methoxy-5,8-dioxo-6-methyl-9-phenyloxycarbonyloxymethyl-2,3,5,8-tetrahydro-1H-pyrrolo<1,2-a>indol

Base Information

Chemical Name:7-Methoxy-5,8-dioxo-6-methyl-9-phenyloxycarbonyloxymethyl-2,3,5,8-tetrahydro-1H-pyrrolo<1,2-a>indol
CAS No.:4400-23-1
Molecular Formula:C₂₁H₁₉NO₆
Molecular Weight:381.385
Hs Code.:

Synonyms:

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Chemical Property of 7-Methoxy-5,8-dioxo-6-methyl-9-phenyloxycarbonyloxymethyl-2,3,5,8-tetrahydro-1H-pyrrolo<1,2-a>indol

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Technology Process of 7-Methoxy-5,8-dioxo-6-methyl-9-phenyloxycarbonyloxymethyl-2,3,5,8-tetrahydro-1H-pyrrolo<1,2-a>indol

There total 19 articles about 7-Methoxy-5,8-dioxo-6-methyl-9-phenyloxycarbonyloxymethyl-2,3,5,8-tetrahydro-1H-pyrrolo<1,2-a>indol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3420-02-8
6-methylindole

: 4400-23-1
7-Methoxy-5,8-dioxo-6-methyl-9-phenyloxycarbonyloxymethyl-2,3,5,8-tetrahydro-1H-pyrrolo<1,2-a>indol

Guidance literature:: Multi-step reaction with 18 steps

1: 1.) NaH / 1.) DMF, 2.) DMF

2: diethyl ether

3: tetrachloroethene / 120 °C

5: 1 N NaOH / methanol

6: pyridine

7: 90 percent / n-BuLi / tetrahydrofuran

8: 76 percent / AlCl₃ / 1,2-dichloro-ethane

9: m-chloroperoxybenzoic acid (m-CPBA), Na₂HPO₄ / CHCl₃

10: 1 N NaOH / methanol

11: 36 percent / Fremy's salt 3K)2> / acetone; H₂O

12: H₂ / 10percent Pd/C

13: K₂CO₃ / dimethylformamide

14: 55 percent / Fremy's salt 3K)2>

15: H₂ / Pd/C

16: LiAlH₄

17: FeCl₃

18: pyridine

With pyridine; sodium hydroxide; disodium hydrogenphosphate; lithium aluminium tetrahydride; n-butyllithium; aluminium trichloride; potassium nitrososulfonate; hydrogen; iron(III) chloride; sodium hydride; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; sodium hydroxide; palladium on activated charcoal; In tetrahydrofuran; methanol; 1,1,2,2-tetrachloroethylene; diethyl ether; chloroform; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetone;

Reference yield:

: 112291-05-1
Acetic acid 3-(6-methyl-indol-1-yl)-propyl ester

: 4400-23-1
7-Methoxy-5,8-dioxo-6-methyl-9-phenyloxycarbonyloxymethyl-2,3,5,8-tetrahydro-1H-pyrrolo<1,2-a>indol

Guidance literature:: Multi-step reaction with 17 steps

1: diethyl ether

2: tetrachloroethene / 120 °C

4: 1 N NaOH / methanol

5: pyridine

6: 90 percent / n-BuLi / tetrahydrofuran

7: 76 percent / AlCl₃ / 1,2-dichloro-ethane

8: m-chloroperoxybenzoic acid (m-CPBA), Na₂HPO₄ / CHCl₃

9: 1 N NaOH / methanol

10: 36 percent / Fremy's salt 3K)2> / acetone; H₂O

11: H₂ / 10percent Pd/C

12: K₂CO₃ / dimethylformamide

13: 55 percent / Fremy's salt 3K)2>

14: H₂ / Pd/C

15: LiAlH₄

16: FeCl₃

17: pyridine

With pyridine; sodium hydroxide; disodium hydrogenphosphate; lithium aluminium tetrahydride; n-butyllithium; aluminium trichloride; potassium nitrososulfonate; hydrogen; iron(III) chloride; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; sodium hydroxide; palladium on activated charcoal; In tetrahydrofuran; methanol; 1,1,2,2-tetrachloroethylene; diethyl ether; chloroform; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetone;

Reference yield:

: 112291-02-8
methyl 6-methyl-2,3-dihydro-1H-pyrrolo[1,2-a]indole-9-carboxylate

: 4400-23-1
7-Methoxy-5,8-dioxo-6-methyl-9-phenyloxycarbonyloxymethyl-2,3,5,8-tetrahydro-1H-pyrrolo<1,2-a>indol

Guidance literature:: Multi-step reaction with 11 steps

1: 76 percent / AlCl₃ / 1,2-dichloro-ethane

2: m-chloroperoxybenzoic acid (m-CPBA), Na₂HPO₄ / CHCl₃

3: 1 N NaOH / methanol

4: 36 percent / Fremy's salt 3K)2> / acetone; H₂O

5: H₂ / 10percent Pd/C

6: K₂CO₃ / dimethylformamide

7: 55 percent / Fremy's salt 3K)2>

8: H₂ / Pd/C

9: LiAlH₄

10: FeCl₃

11: pyridine

With pyridine; sodium hydroxide; disodium hydrogenphosphate; lithium aluminium tetrahydride; aluminium trichloride; potassium nitrososulfonate; hydrogen; iron(III) chloride; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; palladium on activated charcoal; In methanol; chloroform; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetone;