(Z)-7-[(1R,2R,3R,5S)-3,5-Bis-trimethylsilanyloxy-2-((E)-(S)-3-trimethylsilanyloxy-oct-1-enyl)-cyclopentyl]-hept-5-enoic acid pentafluorophenylmethyl ester

Base Information

• Chemical Name: (Z)-7-[(1R,2R,3R,5S)-3,5-Bis-trimethylsilanyloxy-2-((E)-(S)-3-trimethylsilanyloxy-oct-1-enyl)-cyclopentyl]-hept-5-enoic acid pentafluorophenylmethyl ester
• CAS No.: 50673-38-6
• Molecular Formula: C₃₆H₅₉F₅O₅Si₃
• Molecular Weight: 751.11

Synonyms:

Chemical Property of (Z)-7-[(1R,2R,3R,5S)-3,5-Bis-trimethylsilanyloxy-2-((E)-(S)-3-trimethylsilanyloxy-oct-1-enyl)-cyclopentyl]-hept-5-enoic acid pentafluorophenylmethyl ester

Chemical Property:

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Useful:

Technology Process of (Z)-7-[(1R,2R,3R,5S)-3,5-Bis-trimethylsilanyloxy-2-((E)-(S)-3-trimethylsilanyloxy-oct-1-enyl)-cyclopentyl]-hept-5-enoic acid pentafluorophenylmethyl ester

There total 2 articles about (Z)-7-[(1R,2R,3R,5S)-3,5-Bis-trimethylsilanyloxy-2-((E)-(S)-3-trimethylsilanyloxy-oct-1-enyl)-cyclopentyl]-hept-5-enoic acid pentafluorophenylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N,O-Bis(trimethylsilyl)trifluoroacetamide (25561-30-2) + (Z)-7-[(3R,5S)-3,5-Dihydroxy-2-((E)-3-hydroxy-oct-1-enyl)-cyclopentyl]-hept-5-enoic acid pentafluorophenylmethyl ester → (Z)-7-[(1R,2R,3R,5S)-3,5-Bis-trimethylsilanyloxy-2-((E)-(S)-3-trimethylsilanyloxy-oct-1-enyl)-cyclopentyl]-hept-5-enoic acid pentafluorophenylmethyl ester (50673-38-6) + (Z)-7-[(1S,2R,3R,5S)-3,5-Bis-trimethylsilanyloxy-2-((E)-(S)-3-trimethylsilanyloxy-oct-1-enyl)-cyclopentyl]-hept-5-enoic acid pentafluorophenylmethyl ester + (Z)-7-[(1S,2R,3R,5S)-3,5-Bis-trimethylsilanyloxy-2-((E)-(R)-3-trimethylsilanyloxy-oct-1-enyl)-cyclopentyl]-hept-5-enoic acid pentafluorophenylmethyl ester + (Z)-7-[(1R,2R,3R,5S)-3,5-Bis-trimethylsilanyloxy-2-((E)-(R)-3-trimethylsilanyloxy-oct-1-enyl)-cyclopentyl]-hept-5-enoic acid pentafluorophenylmethyl ester

Guidance literature:

In N,N-dimethyl-formamide; at 40 ℃; for 0.333333h; Further byproducts.;

DOI:10.1021/ja0201092

Reference yield:

→ (Z)-7-[(1R,2R,3R,5S)-3,5-Bis-trimethylsilanyloxy-2-((E)-(S)-3-trimethylsilanyloxy-oct-1-enyl)-cyclopentyl]-hept-5-enoic acid pentafluorophenylmethyl ester (50673-38-6)

Guidance literature:

Prostaglandin-F(2α)-pentafluor-benzylester, N,O-Bis-(trimethylsilyl)-acetamid;

DOI:10.1002/jps.2600620906

upstream raw materials:

N,O-Bis(trimethylsilyl)trifluoroacetamide

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