(7S,9S,10R)-9-Benzyloxymethoxy-7-(tert-butyl-dimethyl-silanyloxy)-11-[(1S,3R,4R)-4-(tert-butyl-dimethyl-silanyloxy)-3-methoxy-cyclohexyl]-10-methyl-undecanoic acid methyl ester

Base Information

Chemical Name:(7S,9S,10R)-9-Benzyloxymethoxy-7-(tert-butyl-dimethyl-silanyloxy)-11-[(1S,3R,4R)-4-(tert-butyl-dimethyl-silanyloxy)-3-methoxy-cyclohexyl]-10-methyl-undecanoic acid methyl ester
CAS No.:137298-98-7
Molecular Formula:C₄₀H₇₄O₇Si₂
Molecular Weight:723.194
Hs Code.:

(7S,9S,10R)-9-Benzyloxymethoxy-7-(tert-butyl-dimethyl-silanyloxy)-11-[(1S,3R,4R)-4-(tert-butyl-dimethyl-silanyloxy)-3-methoxy-cyclohexyl]-10-methyl-undecanoic acid methyl ester

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Chemical Property of (7S,9S,10R)-9-Benzyloxymethoxy-7-(tert-butyl-dimethyl-silanyloxy)-11-[(1S,3R,4R)-4-(tert-butyl-dimethyl-silanyloxy)-3-methoxy-cyclohexyl]-10-methyl-undecanoic acid methyl ester

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Technology Process of (7S,9S,10R)-9-Benzyloxymethoxy-7-(tert-butyl-dimethyl-silanyloxy)-11-[(1S,3R,4R)-4-(tert-butyl-dimethyl-silanyloxy)-3-methoxy-cyclohexyl]-10-methyl-undecanoic acid methyl ester

There total 6 articles about (7S,9S,10R)-9-Benzyloxymethoxy-7-(tert-butyl-dimethyl-silanyloxy)-11-[(1S,3R,4R)-4-(tert-butyl-dimethyl-silanyloxy)-3-methoxy-cyclohexyl]-10-methyl-undecanoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3587-60-8
Benzyloxymethyl chloride

: 137298-98-7
(7S,9S,10R)-9-Benzyloxymethoxy-7-(tert-butyl-dimethyl-silanyloxy)-11-[(1S,3R,4R)-4-(tert-butyl-dimethyl-silanyloxy)-3-methoxy-cyclohexyl]-10-methyl-undecanoic acid methyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 1) t-BuOOH, 2) DIPEA / 1) V(O)acac2 / 1) CH₂Cl₂, 2) CH₂Cl₂

2: CuCN / diethyl ether / -40 - -20 °C

3: 2,6-lutidine / CH₂Cl₂

5: diethyl ether

With 2,6-dimethylpyridine; tert.-butylhydroperoxide; N-ethyl-N,N-diisopropylamine; bis(acetylacetonate)oxovanadium; In diethyl ether; dichloromethane;
DOI:10.1016/S0040-4039(00)92266-4

Reference yield:

: 131719-87-4
(2R,3S)-1-[(1S,3R,4R)-4-(tert-Butyl-dimethyl-silanyloxy)-3-methoxy-cyclohexyl]-2-methyl-hex-5-en-3-ol

: 137298-98-7
(7S,9S,10R)-9-Benzyloxymethoxy-7-(tert-butyl-dimethyl-silanyloxy)-11-[(1S,3R,4R)-4-(tert-butyl-dimethyl-silanyloxy)-3-methoxy-cyclohexyl]-10-methyl-undecanoic acid methyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 1) t-BuOOH, 2) DIPEA / 1) V(O)acac2 / 1) CH₂Cl₂, 2) CH₂Cl₂

2: CuCN / diethyl ether / -40 - -20 °C

3: 2,6-lutidine / CH₂Cl₂

5: diethyl ether

With 2,6-dimethylpyridine; tert.-butylhydroperoxide; N-ethyl-N,N-diisopropylamine; bis(acetylacetonate)oxovanadium; In diethyl ether; dichloromethane;
DOI:10.1016/S0040-4039(00)92266-4

Reference yield:

: 137298-96-5,137332-25-3
[(1R,2R,4S)-4-((2R,3S)-3-Benzyloxymethoxy-2-methyl-4-oxiranyl-butyl)-2-methoxy-cyclohexyloxy]-tert-butyl-dimethyl-silane

: 137298-98-7
(7S,9S,10R)-9-Benzyloxymethoxy-7-(tert-butyl-dimethyl-silanyloxy)-11-[(1S,3R,4R)-4-(tert-butyl-dimethyl-silanyloxy)-3-methoxy-cyclohexyl]-10-methyl-undecanoic acid methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: CuCN / diethyl ether / -40 - -20 °C

2: 2,6-lutidine / CH₂Cl₂

4: diethyl ether

With 2,6-dimethylpyridine; In diethyl ether; dichloromethane;
DOI:10.1016/S0040-4039(00)92266-4