methyl <α-(dichlorophosphinyl)benzyl>carbamate

Base Information

Chemical Name:methyl <α-(dichlorophosphinyl)benzyl>carbamate
CAS No.:74732-29-9
Molecular Formula:C₉H₁₀Cl₂NO₃P
Molecular Weight:282.063
Hs Code.:

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Chemical Property of methyl <α-(dichlorophosphinyl)benzyl>carbamate

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Technology Process of methyl <α-(dichlorophosphinyl)benzyl>carbamate

There total 5 articles about methyl <α-(dichlorophosphinyl)benzyl>carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 30122-00-0
α-chloro-benzylisocyanate

: 74732-29-9
methyl <α-(dichlorophosphinyl)benzyl>carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: 44 percent / anhydrous FeCl₃ / 1 h / 70 - 80 °C

2: 45 percent / diethyl ether / 1.) 3 h; 2.) overnight

With iron(III) chloride; In diethyl ether;

Reference yield:

: 33054-04-5
phenylacetyl azide

: 74732-29-9
methyl <α-(dichlorophosphinyl)benzyl>carbamate

Guidance literature:: Multi-step reaction with 4 steps

1: toluene / 110 °C

2: 65 percent / sulfuryl chloride, azobisisobutyronitrile / 7 h / 70 - 90 °C

3: 44 percent / anhydrous FeCl₃ / 1 h / 70 - 80 °C

4: 45 percent / diethyl ether / 1.) 3 h; 2.) overnight

With sulfuryl dichloride; 2,2'-azobis(isobutyronitrile); iron(III) chloride; In diethyl ether; toluene;

Reference yield:

: 3173-56-6
benzyl isothiocyanate

: 74732-29-9
methyl <α-(dichlorophosphinyl)benzyl>carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: 65 percent / sulfuryl chloride, azobisisobutyronitrile / 7 h / 70 - 90 °C

2: 44 percent / anhydrous FeCl₃ / 1 h / 70 - 80 °C

3: 45 percent / diethyl ether / 1.) 3 h; 2.) overnight

With sulfuryl dichloride; 2,2'-azobis(isobutyronitrile); iron(III) chloride; In diethyl ether;