Technology Process of C26H27N5O5S
There total 8 articles about C26H27N5O5S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sulphamoyl chloride; triethylamine;
In
dichloromethane;
DOI:10.1021/jm030025j
- Guidance literature:
-
Multi-step reaction with 8 steps
1: n-BuLi / tetrahydrofuran / -78 °C
2: NaBH4 / methanol / 20 °C
3: CBr4; PPh3 / CH2Cl2
4: NaH / tetrahydrofuran
5: HCl / ethyl acetate
6: EDC; HOBT; Et3N / dimethylformamide / 20 °C
7: HCl / ethyl acetate / 20 °C
8: sulfamoyl chloride; Et3N / CH2Cl2
With
hydrogenchloride; sodium tetrahydroborate; n-butyllithium; carbon tetrabromide; sulphamoyl chloride; sodium hydride; benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine; triphenylphosphine;
In
tetrahydrofuran; methanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/jm030025j
- Guidance literature:
-
Multi-step reaction with 7 steps
1: NaBH4 / methanol / 20 °C
2: CBr4; PPh3 / CH2Cl2
3: NaH / tetrahydrofuran
4: HCl / ethyl acetate
5: EDC; HOBT; Et3N / dimethylformamide / 20 °C
6: HCl / ethyl acetate / 20 °C
7: sulfamoyl chloride; Et3N / CH2Cl2
With
hydrogenchloride; sodium tetrahydroborate; carbon tetrabromide; sulphamoyl chloride; sodium hydride; benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine; triphenylphosphine;
In
tetrahydrofuran; methanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/jm030025j