trans-Pd(COPh)(Br)(PMePh₂)2

Base Information

Chemical Name:trans-Pd(COPh)(Br)(PMePh₂)2
CAS No.:89177-97-9
Molecular Formula:C₃₃H₃₁BrOP₂Pd
Molecular Weight:691.88
Hs Code.:

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Chemical Property of trans-Pd(COPh)(Br)(PMePh₂)2

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Technology Process of trans-Pd(COPh)(Br)(PMePh₂)2

There total 2 articles about trans-Pd(COPh)(Br)(PMePh₂)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: trans-PdEt₂(PMePh₂)2

: 618-32-6
Benzoyl bromide

: 89177-97-9
trans-Pd(COPh)(Br)(PMePh₂)2

Guidance literature:: With styrene; In toluene; styrene and toluene were added to a cooled to -30°C Schlenk tube containing Pd-complex, mixt. was allowed to warm to room temp. during 2 h, PhCOBr was added; ppt. was filtered, washed with Et2O, dried in vacuo, recrystd. from CH2Cl2-hexane; elem. anal.;

Reference yield:

: trans-PdEt₂(PMePh₂)2

: 89177-96-8
2-oxo-2-phenylacetyl bromide

: 89177-97-9
trans-Pd(COPh)(Br)(PMePh₂)2

: trans-Pd(COCOPh)Br(PMePh₂)2

Guidance literature:: With styrene; In toluene; byproducts: CO; toluene and styrene were added to Pd-complex under inert atm., mixt. was stirred at room temp. yielding a homogeneous soln., soln. was cooled to -70°C, PhCOCOBr was added, mixt. was stirred for at -70°C; 1 equiv of CO evolved;