chloro[methoxy(2-phenylthiazol-5-yl)methylidene]gold

Base Information

Chemical Name:chloro[methoxy(2-phenylthiazol-5-yl)methylidene]gold
CAS No.:1225285-33-5
Molecular Formula:C₁₁H₉AuClNOS
Molecular Weight:435.684
Hs Code.:

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Chemical Property of chloro[methoxy(2-phenylthiazol-5-yl)methylidene]gold

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Technology Process of chloro[methoxy(2-phenylthiazol-5-yl)methylidene]gold

There total 4 articles about chloro[methoxy(2-phenylthiazol-5-yl)methylidene]gold which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 39929-21-0
(tetrahydrothiophene)gold(I) chloride

: pentacarbonyl[methoxy(2-phenylthiazol-5-yl)methylidene]tungsten

: 1225285-33-5
chloro[methoxy(2-phenylthiazol-5-yl)methylidene]gold

Guidance literature:: In tetrahydrofuran; (Ar); std. Schlenk technique; Au complex was added to soln. of W complexin THF at -5°C; stirred for 1 h while warmed to 5°C; evapd. (vac.); redissolved in CH2Cl2; filtered; layered with hexane; stored at -20°C; elem. anal.;
DOI:10.1039/b9nj00413k

Reference yield:

: 1826-11-5
2-phenylthiazole

: 1225285-33-5
chloro[methoxy(2-phenylthiazol-5-yl)methylidene]gold

Guidance literature:: Multi-step reaction with 4 steps

1: BuLi / tetrahydrofuran; hexane

2: dichloromethane; water

3: acetonitrile; dichloromethane

4: tetrahydrofuran

With BuLi; In tetrahydrofuran; hexane; dichloromethane; water; acetonitrile;
DOI:10.1039/b9nj00413k

Reference yield:

: 1225285-45-9
lithium pentacarbonyl[(2-phenylthiazol-5-yl)carbonyl]tungstate

: 1225285-33-5
chloro[methoxy(2-phenylthiazol-5-yl)methylidene]gold

Guidance literature:: Multi-step reaction with 3 steps

1: dichloromethane; water

2: acetonitrile; dichloromethane

3: tetrahydrofuran

In tetrahydrofuran; dichloromethane; water; acetonitrile;
DOI:10.1039/b9nj00413k