Technology Process of tert-butyl 4-nitrophenylacetylenyl ether
There total 4 articles about tert-butyl 4-nitrophenylacetylenyl ether which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
In
N,N-dimethyl-formamide;
at 0 ℃;
for 0.333333h;
Inert atmosphere;
DOI:10.1002/chem.201203015
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium periodate; ruthenium trichloride / water; acetonitrile; ethyl acetate / 0 °C
2: N,N-dimethyl-formamide / 0.33 h / 0 °C / Inert atmosphere
With
ruthenium trichloride; sodium periodate;
In
water; ethyl acetate; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/chem.201203015
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.17 h / -78 °C / Inert atmosphere
1.2: 0.33 h / -78 °C / Inert atmosphere
2.1: sodium periodate; ruthenium trichloride / water; acetonitrile; ethyl acetate / 0 °C
3.1: N,N-dimethyl-formamide / 0.33 h / 0 °C / Inert atmosphere
With
ruthenium trichloride; sodium periodate; potassium hexamethylsilazane;
In
tetrahydrofuran; water; ethyl acetate; N,N-dimethyl-formamide; toluene; acetonitrile;
DOI:10.1002/chem.201203015
