Technology Process of 2-(2-aminoethoxy)ethyl-9-hydroxy-6-methylellipticinium chloride
There total 10 articles about 2-(2-aminoethoxy)ethyl-9-hydroxy-6-methylellipticinium chloride which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 9 steps
1: benzene / 2 h / Reflux
2: sodium tetrahydroborate / methanol / 2 h / 20 °C
3: pyridine / acetonitrile / 8 h / 20 °C
4: hydrogenchloride / 1,4-dioxane / 3 h / 130 °C
5: hexamethylenetetramine / 0.33 h / Reflux
6: sulfuric acid; dihydrogen peroxide / methanol / 4 h / Reflux
7: N,N-dimethyl-formamide / 12 h / 80 °C
8: Amberlite? IRA-900 (chloride form) / water / 5 h / 20 °C
9: hydrogenchloride / water / 5 h / 20 °C
With
pyridine; hydrogenchloride; sodium tetrahydroborate; hexamethylenetetramine; sulfuric acid; dihydrogen peroxide;
In
1,4-dioxane; methanol; water; N,N-dimethyl-formamide; acetonitrile; benzene;
6: |Dakin Phenol Oxidation;
DOI:10.1016/j.ejmech.2014.05.032
- Guidance literature:
-
Multi-step reaction with 6 steps
1: hydrogenchloride / 1,4-dioxane / 3 h / 130 °C
2: hexamethylenetetramine / 0.33 h / Reflux
3: sulfuric acid; dihydrogen peroxide / methanol / 4 h / Reflux
4: N,N-dimethyl-formamide / 12 h / 80 °C
5: Amberlite? IRA-900 (chloride form) / water / 5 h / 20 °C
6: hydrogenchloride / water / 5 h / 20 °C
With
hydrogenchloride; hexamethylenetetramine; sulfuric acid; dihydrogen peroxide;
In
1,4-dioxane; methanol; water; N,N-dimethyl-formamide;
3: |Dakin Phenol Oxidation;
DOI:10.1016/j.ejmech.2014.05.032
