1-methoxy-2-phenyl cycylopropane

Base Information

• Chemical Name: 1-methoxy-2-phenyl cycylopropane
• CAS No.: 26269-57-8
• Molecular Formula: C₁₀H₁₂O
• Molecular Weight: 148.205
• Mol file: 26269-57-8.mol

Synonyms:

Chemical Property of 1-methoxy-2-phenyl cycylopropane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-methoxy-2-phenyl cycylopropane

There total 5 articles about 1-methoxy-2-phenyl cycylopropane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

styrene (100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6) + Dichloromethyl methyl ether (4885-02-3) → 1-methoxy-2-phenyl cycylopropane (26269-57-8,50795-01-2)

Guidance literature:

With methyllithium; In diethyl ether;

Reference yield:

styrene (100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6) + Dichloromethyl methyl ether (4885-02-3) → trans-1-methoxy-2-phenylcyclopropane (26269-57-8,50795-01-2)

Guidance literature:

With methyllithium;

DOI:10.1021/jo00837a604

Reference yield:

diiodomethane (75-11-6) + 1-(2-methoxyvinyl)benzene (4747-15-3) → trans-1-methoxy-2-phenylcyclopropane (26269-57-8,50795-01-2) + cis-1-methoxy-2-phenylcyclopropane

Guidance literature:

With zinc silver; Yield given. Multistep reaction. Yields of byproduct given; 1.) diethyl ether, 2 h, 2.) reflux, overnight;

upstream raw materials:

styrene

Dichloromethyl methyl ether

diiodomethane

1-(2-methoxyvinyl)benzene

Downstream raw materials:

3-methoxy-3-phenyl-propionaldehyde dimethylacetal