5,6-dihydro-3-methoxybenzanthracene-7,12-dione

• Chemical Name: 5,6-dihydro-3-methoxybenzanthracene-7,12-dione
• Molecular Formula: C₁₉H₁₄O₃
• Molecular Weight: 290.318
• Mol file: 72428-44-5.mol

Synonyms:

Chemical Property of 5,6-dihydro-3-methoxybenz

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 5,6-dihydro-3-methoxybenz

There total 1 articles about 5,6-dihydro-3-methoxybenzanthracene-7,12-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 21.0%

3-methoxystyrene (626-20-0) + [1,4]naphthoquinone (130-15-4) → 3-methoxybenzanthracene-7,12-dione (63216-11-5) + 5,6-dihydro-3-methoxybenzanthracene-7,12-dione (72428-44-5)

Guidance literature:

With chloranil; trichloroacetic acid; In toluene; at 105 ℃; for 288h;

DOI:10.1021/jo01292a041

Reference yield: 87.0%

5,6-dihydro-3-methoxybenzanthracene-7,12-dione (72428-44-5) → 3-methoxybenzanthracene-7,12-dione (63216-11-5)

Guidance literature:

With potassium hydroxide; oxygen; In ethanol; for 3h;

DOI:10.1021/jo01292a041

upstream raw materials:

3-methoxystyrene

[1,4]naphthoquinone

Downstream raw materials:

3-methoxybenzanthracene-7,12-dione