N-(6-chloronicotinoyl)-γ-aminobutyric acid sodium salt

Base Information

• Chemical Name: N-(6-chloronicotinoyl)-γ-aminobutyric acid sodium salt
• CAS No.: 1352942-06-3
• Molecular Formula: C₁₀H₁₀ClN₂O₃*Na
• Molecular Weight: 264.644
• Mol file: 1352942-06-3.mol

Synonyms:

Chemical Property of N-(6-chloronicotinoyl)-γ-aminobutyric acid sodium salt

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of N-(6-chloronicotinoyl)-γ-aminobutyric acid sodium salt

There total 2 articles about N-(6-chloronicotinoyl)-γ-aminobutyric acid sodium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

N-(6-chloronicotinoyl)-γ-aminobutyric acid (1094685-81-0) → N-(6-chloronicotinoyl)-γ-aminobutyric acid sodium salt (1352942-06-3)

Guidance literature:

With sodium hydroxide; In methanol;

DOI:10.1007/s10600-011-0057-4

Reference yield:

6-Chloronicotinoyl chloride (58757-38-3) → N-(6-chloronicotinoyl)-γ-aminobutyric acid sodium salt (1352942-06-3)

Guidance literature:

Multi-step reaction with 2 steps

1.1: sodium hydroxide / water / -7 - -5 °C

1.2: 1 h / -7 - -5 °C / pH Ca_. 1 - 2

2.1: sodium hydroxide / methanol

With sodium hydroxide; In methanol; water; 1.1: Schotten-Baumann reaction;

DOI:10.1007/s10600-011-0057-4

upstream raw materials:

6-Chloronicotinoyl chloride

N-(6-chloronicotinoyl)-γ-aminobutyric acid