trans-1-ethyl-4-propoxycyclohexyl isocyanate

Base Information

Chemical Name:trans-1-ethyl-4-propoxycyclohexyl isocyanate
CAS No.:950772-76-6
Molecular Formula:C₁₂H₂₁NO₂
Molecular Weight:211.304
Hs Code.:

Synonyms:

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Chemical Property of trans-1-ethyl-4-propoxycyclohexyl isocyanate

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of trans-1-ethyl-4-propoxycyclohexyl isocyanate

There total 5 articles about trans-1-ethyl-4-propoxycyclohexyl isocyanate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 950772-72-2
trans-1-ethyl-4-hydroxy-cyclohexanecarboxylic acid ethyl ester

: 950772-76-6
trans-1-ethyl-4-propoxycyclohexyl isocyanate

Guidance literature:: Multi-step reaction with 4 steps

1: 1H-imidazole / N,N-dimethyl-formamide / 20 °C

2: triethylsilane; bismuth(III) bromide / acetonitrile / 0.5 h / 0 - 20 °C

3: sodium hydroxide; water / tetrahydrofuran; methanol / 50 °C

4: diphenyl phosphoryl azide; triethylamine / toluene / 0.5 h / 100 °C

With 1H-imidazole; triethylsilane; sodium hydroxide; diphenyl phosphoryl azide; water; bismuth(III) bromide; triethylamine; In tetrahydrofuran; methanol; N,N-dimethyl-formamide; toluene; acetonitrile;

Reference yield:

: 862728-41-4
trans-1-ethyl-4-hydroxy-cyclohexanecarboxylic acid ethyl ester

: 950772-76-6
trans-1-ethyl-4-propoxycyclohexyl isocyanate

Guidance literature:: Multi-step reaction with 6 steps

1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 76 h / 0 - 20 °C

2: potassium carbonate / methanol / 1 h / 20 °C

3: 1H-imidazole / N,N-dimethyl-formamide / 20 °C

4: triethylsilane; bismuth(III) bromide / acetonitrile / 0.5 h / 0 - 20 °C

5: sodium hydroxide; water / tetrahydrofuran; methanol / 50 °C

6: diphenyl phosphoryl azide; triethylamine / toluene / 0.5 h / 100 °C

With 1H-imidazole; triethylsilane; sodium hydroxide; di-isopropyl azodicarboxylate; diphenyl phosphoryl azide; water; bismuth(III) bromide; potassium carbonate; triethylamine; triphenylphosphine; In tetrahydrofuran; methanol; N,N-dimethyl-formamide; toluene; acetonitrile;

Reference yield:

: 950772-71-1
trans-ethyl 1-ethyl-4-(chloroacetoxy)cyclohexanecarboxylate

: 950772-76-6
trans-1-ethyl-4-propoxycyclohexyl isocyanate

Guidance literature:: Multi-step reaction with 5 steps

1: potassium carbonate / methanol / 1 h / 20 °C

2: 1H-imidazole / N,N-dimethyl-formamide / 20 °C

3: triethylsilane; bismuth(III) bromide / acetonitrile / 0.5 h / 0 - 20 °C

4: sodium hydroxide; water / tetrahydrofuran; methanol / 50 °C

5: diphenyl phosphoryl azide; triethylamine / toluene / 0.5 h / 100 °C

With 1H-imidazole; triethylsilane; sodium hydroxide; diphenyl phosphoryl azide; water; bismuth(III) bromide; potassium carbonate; triethylamine; In tetrahydrofuran; methanol; N,N-dimethyl-formamide; toluene; acetonitrile;