Technology Process of diptocarpiline
There total 12 articles about diptocarpiline which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dihydrogen peroxide; acetic acid;
for 1h;
Ambient temperature;
DOI:10.1007/BF00597577
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 95 percent / tributyloctadecylphosphonium bromide / benzene / 4 h / 80 °C
2: 15 percent / dimethylformamide / 24 h / Ambient temperature
3: 1) 85percent N2H4*H2O, 2) aq. HCl / 1) CH3OH, reflux, 15 h, 2) H2O, 100 deg C, 5 h
4: 40 percent / (C2H5)3N / CH2Cl2 / 0.5 h / -20 °C
5: 65 percent / 30percent aq. H2O2, glac. CH3CO2H / 1 h / Ambient temperature
With
hydrogenchloride; dihydrogen peroxide; hydrazine hydrate; acetic acid; triethylamine; octadecyltributylphosphonium bromide;
In
dichloromethane; N,N-dimethyl-formamide; benzene;
DOI:10.1007/BF00597577
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 15 percent / dimethylformamide / 24 h / Ambient temperature
2: 1) 85percent N2H4*H2O, 2) aq. HCl / 1) CH3OH, reflux, 15 h, 2) H2O, 100 deg C, 5 h
3: 40 percent / (C2H5)3N / CH2Cl2 / 0.5 h / -20 °C
4: 65 percent / 30percent aq. H2O2, glac. CH3CO2H / 1 h / Ambient temperature
With
hydrogenchloride; dihydrogen peroxide; hydrazine hydrate; acetic acid; triethylamine;
In
dichloromethane; N,N-dimethyl-formamide;
DOI:10.1007/BF00597577
