2-methyl-1,3-butadiene-1,3,4-tricarboxylic acid monolactone

Base Information

• Chemical Name: 2-methyl-1,3-butadiene-1,3,4-tricarboxylic acid monolactone
• CAS No.: 866017-37-0
• Molecular Formula: C₈H₈O₆
• Molecular Weight: 200.148
• Mol file: 866017-37-0.mol

Synonyms:

Chemical Property of 2-methyl-1,3-butadiene-1,3,4-tricarboxylic acid monolactone

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of 2-methyl-1,3-butadiene-1,3,4-tricarboxylic acid monolactone

There total 1 articles about 2-methyl-1,3-butadiene-1,3,4-tricarboxylic acid monolactone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

glyoxylic acid ethyl ester (924-44-7) + dimethyl 3-methyl-2-cis-pentenedioate (81061-91-8) → 2-methyl-1,3-butadiene-1,3,4-tricarboxylic acid monolactone (866017-37-0) + 2-methyl-(1E,3Z)-butadiene-1,3,4-tricarboxylic acid + 4-methyl-5-carboxymethyl-2-furanone (6307-98-8)

Guidance literature:

With methanol; potassium hydroxide; In toluene; at 20 ℃;

DOI:10.1021/jo0507892

upstream raw materials:

glyoxylic acid ethyl ester

dimethyl 3-methyl-2-cis-pentenedioate