n-butyl-β-D-fructopyranoside

Base Information

• Chemical Name: n-butyl-β-D-fructopyranoside
• CAS No.: 67884-27-9
• Molecular Formula: C₁₀H₂₀O₆
• Molecular Weight: 236.265
• Mol file: 67884-27-9.mol

Synonyms:

Chemical Property of n-butyl-β-D-fructopyranoside

Chemical Property:

• Melting Point: 152-154 °C
• Boiling Point: 405.6±45.0 °C(Predicted)
• PKA: 12.83±0.70(Predicted)
• Density: 1.31±0.1 g/cm3(Predicted)

Purity/Quality:

HPLC≥98% ^*data from raw suppliers

n-Butyl-β-D-fructopyranoside 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of n-butyl-β-D-fructopyranoside

There total 7 articles about n-butyl-β-D-fructopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

but-2-enyl β-D-fructopyranoside → n-butyl β-D-fructopyranoside (78008-09-0,93590-02-4,67884-27-9)

Guidance literature:

With hydrogen; triethylamine; palladium on activated charcoal; In water; at 20 ℃; for 6h; under 760 Torr;

DOI:10.1016/j.carres.2006.02.005

Reference yield: 42.4%

fructopyranose (6347-01-9) + butan-1-ol (71-36-3) → n-butyl β-D-fructopyranoside (78008-09-0,93590-02-4,67884-27-9) + α-D-fructofuranose 2-butyl ether (80971-59-1)

Guidance literature:

With hydrogenchloride; for 20h; Ambient temperature;

DOI:10.1021/jm00354a021

Reference yield: 41.0%

4'-Chlorobutyl β-D-fructopyranoside → n-butyl β-D-fructopyranoside (78008-09-0,93590-02-4,67884-27-9)

Guidance literature:

With hydrogen; sodium hydrogencarbonate; palladium on activated charcoal; In water; at 45 - 50 ℃;

DOI:10.1002/recl.19931120906

upstream raw materials:

fructopyranose

butan-1-ol

D-fructose

D-Fructose

Refernces

• 1、 De Goede,Van Deurzen,Van Der Leij,Van Der Heijden,Baas,Van Rantwijk,Van Bekkum. "Synthesis of alkyl fructosides using solid acid catalysts. Part I: Silica-alumina cracking catalysts". . p. 331 - 349. Retrieved 1996.
• 2、 Van Der Heijden,Van Rantwijk,Van Bekkum. "MCM-41 materials as catalysts for the synthesis of alkyl fructosides". . p. 131 - 147. Retrieved 2007/10/03.