1,3-Dimethyl-1H-cyclopenta-1,2,4-triazin-5,7-dicarbonsaeure-dimethylester

Base Information

Chemical Name:1,3-Dimethyl-1H-cyclopenta-1,2,4-triazin-5,7-dicarbonsaeure-dimethylester
CAS No.:83274-39-9
Molecular Formula:C₁₂H₁₃N₃O₄
Molecular Weight:263.253
Hs Code.:

1,3-Dimethyl-1H-cyclopenta<e>-1,2,4-triazin-5,7-dicarbonsaeure-dimethylester

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Chemical Property of 1,3-Dimethyl-1H-cyclopenta-1,2,4-triazin-5,7-dicarbonsaeure-dimethylester

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Technology Process of 1,3-Dimethyl-1H-cyclopenta-1,2,4-triazin-5,7-dicarbonsaeure-dimethylester

There total 5 articles about 1,3-Dimethyl-1H-cyclopenta-1,2,4-triazin-5,7-dicarbonsaeure-dimethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 27.0%

: 83274-26-4
3-Methyl-4H-cyclopenta-1,2,4-triazin-5,7-dicarbonsaeure-dimethylester

: 77-78-1
dimethyl sulfate

: 83274-40-2
2,3-Dimethyl-2H-cyclopenta-1,2,4-triazin-5,7-dicarbonsaeure-dimethylester

: 83274-39-9
1,3-Dimethyl-1H-cyclopenta-1,2,4-triazin-5,7-dicarbonsaeure-dimethylester

Guidance literature:: With triethylamine; In methanol; for 48h; Ambient temperature;

Reference yield: 15.0%

: 83274-26-4
3-Methyl-4H-cyclopenta-1,2,4-triazin-5,7-dicarbonsaeure-dimethylester

: 77-78-1
dimethyl sulfate

: 83274-40-2
2,3-Dimethyl-2H-cyclopenta-1,2,4-triazin-5,7-dicarbonsaeure-dimethylester

: 83274-39-9
1,3-Dimethyl-1H-cyclopenta-1,2,4-triazin-5,7-dicarbonsaeure-dimethylester

Guidance literature:: With triethylamine; In methanol; for 48h; Ambient temperature;

Reference yield:

: 1119-40-0
Dimethyl glutarate

: 83274-39-9
1,3-Dimethyl-1H-cyclopenta-1,2,4-triazin-5,7-dicarbonsaeure-dimethylester

Guidance literature:: Multi-step reaction with 4 steps

1: 60 percent

2: 50 percent / Et₃N / methanol / 1) reflux, 30 min, 2) r.t., 3 d

3: 52 percent / NaNO₂ / formic acid / CH₃COOH

4: 27 percent / Et₃N / methanol / 48 h / Ambient temperature

With triethylamine; sodium nitrite; In methanol; formic acid;