8-acetyl-4-methyl-9-phenyl-2H-furo[2,3-h]chromen-2-one

Base Information

• Chemical Name: 8-acetyl-4-methyl-9-phenyl-2H-furo[2,3-h]chromen-2-one
• CAS No.: 6083-69-8
• Molecular Formula: C₉H₈N₂O₇
• Molecular Weight: 256.172
• DSSTox Substance ID: DTXSID90976301
• Wikidata: Q82961134
• ChEMBL ID: CHEMBL600015
• Mol file: 6083-69-8.mol

Synonyms:8-acetyl-4-methyl-9-phenyl-2H-furo[2,3-h]chromen-2-one;6083-69-8;CBMicro_019078;ChemDiv1_024493;CHEMBL600015;SCHEMBL10038082;HMS656J07;DTXSID90976301;CCG-13857;STK856433;AKOS001640565;BIM-0019179.P001;SR-01000483304;SR-01000483304-1;8-Acetyl-4-methyl-9-phenyl-2H-furo[2,3-h][1]benzopyran-2-one

Chemical Property of 8-acetyl-4-methyl-9-phenyl-2H-furo[2,3-h]chromen-2-one

Chemical Property:

• Vapor Pressure: 7.79E-12mmHg at 25°C
• XLogP3: 3.9
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 2
• Exact Mass: 318.08920892
• Heavy Atom Count: 24
• Complexity: 560

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: CC1=CC(=O)OC2=C1C=CC3=C2C(=C(O3)C(=O)C)C4=CC=CC=C4

Technology Process of 8-acetyl-4-methyl-9-phenyl-2H-furo[2,3-h]chromen-2-one

There total 17 articles about 8-acetyl-4-methyl-9-phenyl-2H-furo[2,3-h]chromen-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-fluoro-3,5-dinitrobenzoic acid (445-65-8) → 2-Ethoxy-3,5-dinitro-benzoesaeure (6083-69-8)

Guidance literature:

With potassium hydroxide;

DOI:10.1002/hlca.19540370419

Reference yield:

→ 2-Ethoxy-3,5-dinitro-benzoesaeure (6083-69-8)

Guidance literature:

With permanganate(VII) ion;

Reference yield:

o-fluoro-benzoic acid (445-29-4) → 2-Ethoxy-3,5-dinitro-benzoesaeure (6083-69-8)

Guidance literature:

Multi-step reaction with 2 steps

2: ethanolic KOH

With potassium hydroxide;

DOI:10.1002/hlca.19540370419

upstream raw materials:

ethanol

2-chloro-3,5-dinitrobenzoic acid

2,3,5-trinitro-benzoic acid

2-fluoro-3,5-dinitrobenzoic acid