cis-1-bromo-2,2-dimethyl-3-vinylcyclopropane

Base Information

Chemical Name:cis-1-bromo-2,2-dimethyl-3-vinylcyclopropane
CAS No.:67885-79-4
Molecular Formula:C₇H₁₁Br
Molecular Weight:175.068
Hs Code.:

Synonyms:

Suppliers and Price of cis-1-bromo-2,2-dimethyl-3-vinylcyclopropane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of cis-1-bromo-2,2-dimethyl-3-vinylcyclopropane

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of cis-1-bromo-2,2-dimethyl-3-vinylcyclopropane

There total 15 articles about cis-1-bromo-2,2-dimethyl-3-vinylcyclopropane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 54105-78-1
1-[(tetrahydro-2H-pyran-2-yl)oxy]-3-methyl-2-butene

: 67885-78-3,67885-79-4
trans-1-bromo-2,2-dimethyl-3-vinylcyclopropane

Guidance literature:: Multi-step reaction with 4 steps

1: 50percent aqueous sodium hydroxide / benzyltriethylammonium chloride / ethanol / 4 h

2: 1.) pyridium chlorochromate, 2.) basic alumina column / 1.) dichloromethane, room temp., 2 h.

3: 1.) n-butyllithium / 1.) THF, -78 deg C -> room temp., 30 min., 2.) THF, room temp., 1 h.

4: zinc dust / acetic acid / 3 h / Ambient temperature

With sodium hydroxide; n-butyllithium; basic alumina column; zinc; N-benzyl-N,N,N-triethylammonium chloride; In ethanol; acetic acid;

Reference yield:

: 54105-78-1
1-[(tetrahydro-2H-pyran-2-yl)oxy]-3-methyl-2-butene

: 67885-78-3,67885-79-4
cis-1-bromo-2,2-dimethyl-3-vinylcyclopropane

Guidance literature:: Multi-step reaction with 4 steps

1: 50percent aqueous sodium hydroxide / benzyltriethylammonium chloride / ethanol / 4 h

2: 1.) pyridium chlorochromate, 2.) basic alumina column / 1.) dichloromethane, room temp., 2 h.

3: 1.) n-butyllithium / 1.) THF, -78 deg C -> room temp., 30 min., 2.) THF, room temp., 1 h.

4: zinc dust / acetic acid / 3 h / Ambient temperature

With sodium hydroxide; n-butyllithium; basic alumina column; zinc; N-benzyl-N,N,N-triethylammonium chloride; In ethanol; acetic acid;

Reference yield:

: 67885-75-0
2,2-Dibromo-3,3-dimethylcyclopropylmethyl 2-Tetrahydropyranyl Ether

: 67885-78-3,67885-79-4
trans-1-bromo-2,2-dimethyl-3-vinylcyclopropane

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / 1 N hydrochloric acid / methanol / Ambient temperature

2: 1.) pyridium chlorochromate, 2.) basic alumina column / 1.) dichloromethane, room temp., 2 h.

3: 1.) n-butyllithium / 1.) THF, -78 deg C -> room temp., 30 min., 2.) THF, room temp., 1 h.

4: zinc dust / acetic acid / 3 h / Ambient temperature

With hydrogenchloride; n-butyllithium; basic alumina column; zinc; In methanol; acetic acid;