6,13-Dimethyl-6,13-dihydrodibenzo[b,i]phenazine

Base Information

• Chemical Name: 6,13-Dimethyl-6,13-dihydrodibenzo[b,i]phenazine
• CAS No.: 70782-26-2
• Molecular Formula: C₂₂H₁₈N₂
• Molecular Weight: 310.398
• NSC Number: 92441
• DSSTox Substance ID: DTXSID50293809
• Wikidata: Q82032775
• Mol file: 70782-26-2.mol

Synonyms:70782-26-2;6,13-dimethyl-6,13-dihydrodibenzo[b,i]phenazine;NSC92441;SCHEMBL2330603;DTXSID50293809;NSC-92441

Chemical Property of 6,13-Dimethyl-6,13-dihydrodibenzo[b,i]phenazine

Chemical Property:

• Vapor Pressure: 6.98E-11mmHg at 25°C
• XLogP3: 4.7
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 0
• Exact Mass: 310.146998583
• Heavy Atom Count: 24
• Complexity: 381

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: CN1C2=CC3=CC=CC=C3C=C2N(C4=CC5=CC=CC=C5C=C41)C

Technology Process of 6,13-Dimethyl-6,13-dihydrodibenzo[b,i]phenazine

There total 2 articles about 6,13-Dimethyl-6,13-dihydrodibenzo[b,i]phenazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

6,13-dihydrodibenzophenazine (10350-06-8) + methyl iodide (74-88-4) → 6,13-dimethyl-6,13-dihydrodibenzophenazine (70782-26-2)

Guidance literature:

With lithium diisopropyl amide; In tetrahydrofuran; for 1.5h; Ambient temperature;

DOI:10.1021/ja00521a049

Reference yield:

6,13-dihydrodibenzophenazine (10350-06-8) + methyl iodide (74-88-4) → 6-methyl-6,13-dihydro-6,13-diazapentacene + 6,13-dimethyl-6,13-dihydrodibenzophenazine (70782-26-2)

Guidance literature:

6,13-dihydrodibenzophenazine; With sodium hydride; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 1.33333h; Inert atmosphere;

methyl iodide; In N,N-dimethyl-formamide; at 20 ℃; for 14h; Inert atmosphere; Cooling with ice;

DOI:10.1002/anie.201500684

upstream raw materials:

6,13-dihydrodibenzophenazine

methyl iodide