C₂₇H₄₂O₉P^(1-)*Na⁽¹⁺⁾

Base Information

• Chemical Name: C₂₇H₄₂O₉P^(1-)*Na⁽¹⁺⁾
• CAS No.: 1313387-69-7
• Molecular Formula: C₂₇H₄₂O₉P*Na
• Molecular Weight: 564.589
• Mol file: 1313387-69-7.mol

Synonyms:

Chemical Property of C₂₇H₄₂O₉P^(1-)*Na⁽¹⁺⁾

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₇H₄₂O₉P^(1-)*Na⁽¹⁺⁾

There total 5 articles about C₂₇H₄₂O₉P^(1-)*Na⁽¹⁺⁾ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C36H61O9PSi → C27H42O9P(1-)*Na(1+) (1313387-69-7)

Guidance literature:

C₃₆H₆₁O₉PSi; With hydrogenchloride; In methanol; water; at 20 ℃; for 24h;

With sodium hydrogencarbonate; In methanol; water; for 0.5h; pH=7;

Reference yield:

20-Hydroxyecdysone (5289-74-7) → C27H42O9P(1-)*Na(1+) (1313387-69-7)

Guidance literature:

Multi-step reaction with 6 steps

1.1: N,N-dimethyl-formamide / 8 h / 20 °C

2.1: toluene-4-sulfonic acid / acetone / 12 h / 20 °C

3.1: 1H-imidazole; dmap / dichloromethane / 4 h / 20 °C

4.1: dihydrogen peroxide; sodium hydroxide / dichloromethane / 0.5 h / 20 °C

5.1: pyridine; trichlorophosphate / tetrahydrofuran / 8 h / 20 °C / Cooling with ice

5.2: Cooling with ice

6.1: hydrogenchloride / water; methanol / 24 h / 20 °C

6.2: 0.5 h / pH 7

With pyridine; 1H-imidazole; hydrogenchloride; dmap; dihydrogen peroxide; toluene-4-sulfonic acid; sodium hydroxide; trichlorophosphate; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetone;

Reference yield:

20E 20,22-phenylboronate (142081-57-0) → C27H42O9P(1-)*Na(1+) (1313387-69-7)

Guidance literature:

Multi-step reaction with 5 steps

1.1: toluene-4-sulfonic acid / acetone / 12 h / 20 °C

2.1: 1H-imidazole; dmap / dichloromethane / 4 h / 20 °C

3.1: dihydrogen peroxide; sodium hydroxide / dichloromethane / 0.5 h / 20 °C

4.1: pyridine; trichlorophosphate / tetrahydrofuran / 8 h / 20 °C / Cooling with ice

4.2: Cooling with ice

5.1: hydrogenchloride / water; methanol / 24 h / 20 °C

5.2: 0.5 h / pH 7

With pyridine; 1H-imidazole; hydrogenchloride; dmap; dihydrogen peroxide; toluene-4-sulfonic acid; sodium hydroxide; trichlorophosphate; In tetrahydrofuran; methanol; dichloromethane; water; acetone;

upstream raw materials:

20-Hydroxyecdysone

20E 20,22-phenylboronate

C₃₆H₅₁BO₇

C₄₂H₆₅BO₇Si