dysidin

Base Information

Chemical Name:dysidin
CAS No.:91279-96-8
Molecular Formula:C₁₆H₂₂Cl₃NO₄
Molecular Weight:398.714
Hs Code.:

Synonyms:

Suppliers and Price of dysidin

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of dysidin

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of dysidin

There total 14 articles about dysidin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 133908-08-4
iheyanone

: 1329627-18-0
(5S,E)-6,6,6-trichloro-3-methoxy-5-methylhex-2-enoyl chloride

: 91279-96-8,91279-98-0,95272-90-5,95272-91-6,63079-71-0
dysidin

Guidance literature:: 5-isopropyl-4-methoxy-1,5-dihydro-pyrrol-2-one; With methylmagnesium bromide; In tetrahydrofuran; diethyl ether; at 0 ℃; Inert atmosphere;

(5S,E)-6,6,6-trichloro-3-methoxy-5-methylhex-2-enoyl chloride; In tetrahydrofuran; diethyl ether; at 0 - 25 ℃; for 24h; Inert atmosphere;
DOI:10.1002/asia.201100338

Reference yield:

: 934197-81-6
2-isopropyl-3-methoxy-5-oxo-2,5-dihydro-pyrrole-1-carboxylic acid tert-butyl ester

: 91279-96-8,91279-98-0,95272-90-5,95272-91-6,63079-71-0
dysidin

Guidance literature:: Multi-step reaction with 2 steps

1.1: trifluoroacetic acid / dichloromethane / 0.5 h / 20 - 25 °C / Inert atmosphere

2.1: methylmagnesium bromide / tetrahydrofuran; diethyl ether / 0 °C / Inert atmosphere

2.2: 24 h / 0 - 25 °C / Inert atmosphere

With methylmagnesium bromide; trifluoroacetic acid; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1002/asia.201100338

Reference yield:

: 1207363-08-3
(S)-4,4,4-trichloro-3-methylbutanenitrile

: 91279-96-8,91279-98-0,95272-90-5,95272-91-6,63079-71-0
dysidin

Guidance literature:: Multi-step reaction with 9 steps

1.1: diisobutylaluminium hydride / dichloromethane / 2 h / -78 °C / Inert atmosphere

1.2: 2 h / -78 - 25 °C / Inert atmosphere

2.1: sodium dihydrogenphosphate; sodium chlorite / 2-methyl-but-2-ene; water; tert-butyl alcohol / 3.33 h / 0 - 25 °C / Inert atmosphere

3.1: thionyl chloride; N,N-dimethyl-formamide / dichloromethane / 1 h / Inert atmosphere; Reflux

4.1: pyridine / dichloromethane / 1.5 h / -5 - 25 °C / Inert atmosphere

5.1: 2 h / 65 °C / Inert atmosphere

6.1: N,N,N,N,N,N-hexamethylphosphoric triamide; sodium hydride / mineral oil / 24 h / 5 - 25 °C / Inert atmosphere

7.1: barium hydroxide octahydrate / methanol / 4 h / Inert atmosphere; Reflux

8.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 3 h / 20 - 25 °C / Inert atmosphere

9.1: methylmagnesium bromide / tetrahydrofuran; diethyl ether / 0 °C / Inert atmosphere

9.2: 24 h / 0 - 25 °C / Inert atmosphere

With pyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; sodium chlorite; sodium dihydrogenphosphate; thionyl chloride; oxalyl dichloride; barium hydroxide octahydrate; methylmagnesium bromide; sodium hydride; diisobutylaluminium hydride; N,N-dimethyl-formamide; In tetrahydrofuran; methanol; 2-methyl-but-2-ene; diethyl ether; dichloromethane; water; mineral oil; tert-butyl alcohol;
DOI:10.1002/asia.201100338