ethyl exo-3-(bicyclo<2,2,1>hept-5-en-2-yl)-3-oxopropanoate

Base Information

Chemical Name:ethyl exo-3-(bicyclo<2,2,1>hept-5-en-2-yl)-3-oxopropanoate
CAS No.:56342-58-6
Molecular Formula:C₁₂H₁₆O₃
Molecular Weight:208.257
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl exo-3-(bicyclo<2,2,1>hept-5-en-2-yl)-3-oxopropanoate

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Technology Process of ethyl exo-3-(bicyclo<2,2,1>hept-5-en-2-yl)-3-oxopropanoate

There total 4 articles about ethyl exo-3-(bicyclo<2,2,1>hept-5-en-2-yl)-3-oxopropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₁H₁₂N₂O

: 141-78-6
ethyl acetate

: 56342-58-6,56342-68-8,75275-66-0
ethyl endo-3-(bicyclo<2,2,1>hept-5-en-2-yl)-3-oxopropanoate

: 56342-58-6,56342-68-8,75275-66-0
ethyl exo-3-(bicyclo<2,2,1>hept-5-en-2-yl)-3-oxopropanoate

Guidance literature:: ethyl acetate; With lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃; for 0.5h;

C₁₁H₁₂N₂O; In tetrahydrofuran; at -78 - 23 ℃; for 2.83333h; optical yield given as %de;
DOI:10.1016/j.tet.2010.05.084

Reference yield:

: C₁₁H₁₂N₂O

: 141-78-6
ethyl acetate

: 56342-58-6,56342-68-8,75275-66-0
ethyl endo-3-(bicyclo<2,2,1>hept-5-en-2-yl)-3-oxopropanoate

: 56342-58-6,56342-68-8,75275-66-0
ethyl exo-3-(bicyclo<2,2,1>hept-5-en-2-yl)-3-oxopropanoate

Guidance literature:: ethyl acetate; With lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃; for 0.5h;

C₁₁H₁₂N₂O; In tetrahydrofuran; at -78 - 23 ℃; for 2.83333h; optical yield given as %de;
DOI:10.1016/j.tet.2010.05.084

Reference yield:

: 5063-03-6
2-acetyl-5-norbornene

: 105-58-8,76619-83-5
Diethyl carbonate

: 56342-58-6,56342-68-8,75275-66-0
ethyl endo-3-(bicyclo<2,2,1>hept-5-en-2-yl)-3-oxopropanoate

: 56342-58-6,56342-68-8,75275-66-0
ethyl exo-3-(bicyclo<2,2,1>hept-5-en-2-yl)-3-oxopropanoate

Guidance literature:: With sodium hydride; Multistep reaction. Title compound not separated from byproducts; 1.) THF, reflux, 2.) THF, reflux, 30 min;
DOI:10.1071/CH9820799