2,5-dimethoxy-β,β-dimethoxypropioanilide

Base Information

Chemical Name:2,5-dimethoxy-β,β-dimethoxypropioanilide
CAS No.:75945-51-6
Molecular Formula:C₁₃H₁₉NO₅
Molecular Weight:269.298
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,5-dimethoxy-β,β-dimethoxypropioanilide

Chemical Property:

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Technology Process of 2,5-dimethoxy-β,β-dimethoxypropioanilide

There total 1 articles about 2,5-dimethoxy-β,β-dimethoxypropioanilide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7424-91-1
methyl 3,3-dimethoxypropionate

: 102-56-7,102526-87-4
2,5-dimethoxyaniline

: 75945-51-6
2,5-dimethoxy-β,β-dimethoxypropioanilide

Guidance literature:: With sodium hydroxide; ethyl hydrogen carbonate; Yield given. Multistep reaction; 1.) methanol, room temperature, overnight, 2.) CH₂Cl₂, 30 min, 3.) CH₂Cl₂, reflux, 1 h;
DOI:10.1248/cpb.29.2161

Reference yield:

: 75945-51-6
2,5-dimethoxy-β,β-dimethoxypropioanilide

: 59430-56-7
5,8-Dihydroxy-3,4-dihydro-2(1H)-quinolinone

Guidance literature:: Multi-step reaction with 3 steps

1: 76.3 percent / conc. H₂SO₄ / 1 h / 60 °C

2: 92 percent / H₂ / Raney-Ni / propan-2-ol

3: 80.9 percent / 47percent HBr / 2.5 h / Heating

With sulfuric acid; hydrogen bromide; hydrogen; nickel; In isopropyl alcohol;
DOI:10.1248/cpb.29.2161