1-[Tricyclo[8.2.2.24,7]hexadeca-1(12),4,6,10,13,15-hexaen-5-yl]ethanol

Base Information

Chemical Name:1-[Tricyclo[8.2.2.24,7]hexadeca-1(12),4,6,10,13,15-hexaen-5-yl]ethanol
CAS No.:732-66-1
Molecular Formula:C₁₈H₂₀O
Molecular Weight:252.356
Hs Code.:
NSC Number:34896
DSSTox Substance ID:DTXSID90284019

Synonyms:732-66-1;1-[tricyclo[8.2.2.24,7]hexadeca-1(12),4,6,10,13,15-hexaen-5-yl]ethanol;1-TRICYCLO(8.2.2.2(4,7))HEXADECA-1(13),4,6,10(14),11,15-HEXAEN-5-YL-ETHANOL;NSC34896;DTXSID90284019;NSC-34896;AKOS024323697

Suppliers and Price of 1-[Tricyclo[8.2.2.24,7]hexadeca-1(12),4,6,10,13,15-hexaen-5-yl]ethanol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 1-[Tricyclo[8.2.2.24,7]hexadeca-1(12),4,6,10,13,15-hexaen-5-yl]ethanol

Chemical Property:

Vapor Pressure:1.02E-06mmHg at 25°C
XLogP3:3.9
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:252.151415257
Heavy Atom Count:19
Complexity:279

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C1=C2CCC3=CC=C(CCC(=C1)C=C2)C=C3)O

Technology Process of 1-[Tricyclo[8.2.2.24,7]hexadeca-1(12),4,6,10,13,15-hexaen-5-yl]ethanol

There total 3 articles about 1-[Tricyclo[8.2.2.24,7]hexadeca-1(12),4,6,10,13,15-hexaen-5-yl]ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 10029-00-2
4-acetyl[2.2]paracyclophane

: 732-66-1
(R,S)-methyl-<<2,2>-para-cyclophan-4-yl>carbinol

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 - 20 ℃; for 3h; optical yield given as %de; Inert atmosphere;
DOI:10.1002/ijch.201100079

Reference yield: 59.0%

: 735-65-9
2-bromo-1-tricyclo[8.2.2.24,7]hexadeca-1⁽¹³⁾,4,6,10⁽¹⁴⁾,11,15-hexaen-5-yl-ethanone

: 732-66-1
(R,S)-methyl-<<2,2>-para-cyclophan-4-yl>carbinol

Guidance literature:: With sodium tetrahydroborate; In ethanol; at 70 ℃; for 10h;
DOI:10.1007/BF02219000

Reference yield:

: 1633-22-3
[2.2]Paracyclophan

: 732-66-1
(R,S)-methyl-<<2,2>-para-cyclophan-4-yl>carbinol

Guidance literature:: Multi-step reaction with 2 steps

1: AlCl₃

2: LiAlH₄

With lithium aluminium tetrahydride; aluminium trichloride;
DOI:10.1021/ja00994a014