Technology Process of 3H-Azepin-3-one, hexahydro-1-[(4-methylphenyl)sulfonyl]-5-phenyl-
There total 6 articles about 3H-Azepin-3-one, hexahydro-1-[(4-methylphenyl)sulfonyl]-5-phenyl- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sulfuric acid;
In
diethyl ether;
at 0 ℃;
for 0.0833333h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1) magnesium / 1) diethyl ether, 2) diethyl ether, toluene, RT, 18 h
2: 43 percent / sodium borohydride / ethanol
3: 57 percent / 90 percent sulfuric acid / diethyl ether / 0.08 h / 0 °C
With
sodium tetrahydroborate; sulfuric acid; magnesium;
In
diethyl ether; ethanol;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 34.5 percent / sodium carbonate / H2O; ethanol / 18 h / Heating
2: 86 percent / sodium hydride / tetrahydrofuran / 8 h / Ambient temperature
3: 1) magnesium / 1) diethyl ether, 2) diethyl ether, toluene, RT, 18 h
4: 43 percent / sodium borohydride / ethanol
5: 57 percent / 90 percent sulfuric acid / diethyl ether / 0.08 h / 0 °C
With
sodium tetrahydroborate; sulfuric acid; sodium hydride; sodium carbonate; magnesium;
In
tetrahydrofuran; diethyl ether; ethanol; water;
