4H-Azepin-4-one, 6,6-dichlorohexahydro-1-[(4-methylphenyl)sulfonyl]-

Base Information

Chemical Name:4H-Azepin-4-one, 6,6-dichlorohexahydro-1-[(4-methylphenyl)sulfonyl]-
CAS No.:140160-81-2
Molecular Formula:C13H15Cl2NO3S
Molecular Weight:336.239
Hs Code.:

Synonyms:

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Chemical Property of 4H-Azepin-4-one, 6,6-dichlorohexahydro-1-[(4-methylphenyl)sulfonyl]-

Chemical Property:

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Technology Process of 4H-Azepin-4-one, 6,6-dichlorohexahydro-1-[(4-methylphenyl)sulfonyl]-

There total 5 articles about 4H-Azepin-4-one, 6,6-dichlorohexahydro-1-[(4-methylphenyl)sulfonyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3-[(2-Chloro-allyl)-(toluene-4-sulfonyl)-amino]-propionyl chloride

: 140160-81-2
6,6-dichloro-N-tosylazepan-4-one

Guidance literature:: With aluminium trichloride; In dichloromethane; for 2.5h; Yield given; Ambient temperature;

Reference yield:

: 70-55-3
toluene-4-sulfonamide

: 140160-81-2
6,6-dichloro-N-tosylazepan-4-one

Guidance literature:: Multi-step reaction with 5 steps

1: 34.5 percent / sodium carbonate / H₂O; ethanol / 18 h / Heating

2: 2) sodium hydride / 1) RT, 1 h, 2) RT, 18 h

3: 78 percent / aq. sodium hydroxide / methanol / 24 h / 20 °C

4: thionyl chloride / 18 h / 35 - 40 °C

5: aluminium chloride / CH₂Cl₂ / 2.5 h / Ambient temperature

With sodium hydroxide; aluminium trichloride; thionyl chloride; sodium hydride; sodium carbonate; In methanol; ethanol; dichloromethane; water;

Reference yield:

: 140160-65-2
2-chloro-N-tosylprop-2-enylamine

: 140160-81-2
6,6-dichloro-N-tosylazepan-4-one

Guidance literature:: Multi-step reaction with 4 steps

1: 2) sodium hydride / 1) RT, 1 h, 2) RT, 18 h

2: 78 percent / aq. sodium hydroxide / methanol / 24 h / 20 °C

3: thionyl chloride / 18 h / 35 - 40 °C

4: aluminium chloride / CH₂Cl₂ / 2.5 h / Ambient temperature

With sodium hydroxide; aluminium trichloride; thionyl chloride; sodium hydride; In methanol; dichloromethane;