N'-(4-Chlorobenzylidene)-4-methylbenzenesulfonohydrazide

Base Information

Chemical Name:N'-(4-Chlorobenzylidene)-4-methylbenzenesulfonohydrazide
CAS No.:19350-69-7
Molecular Formula:C14H13 Cl N2 O2 S
Molecular Weight:308.788
Hs Code.:
European Community (EC) Number:651-947-7
NSC Number:338080
DSSTox Substance ID:DTXSID40425915

Synonyms:19350-69-7;N'-(4-Chlorobenzylidene)-4-methylbenzenesulfonohydrazide;NSC338080;N-[(E)-(4-chlorophenyl)methylideneamino]-4-methylbenzenesulfonamide;N'-[(E)-(4-chlorophenyl)methylidene]-4-methylbenzene-1-sulfonohydrazide;N'1-(4-chlorobenzylidene)-4-methylbenzene-1-sulfonohydrazide;SCHEMBL13510934;HMS543O20;DTXSID40425915;AKOS003849388;CCG-234791;NSC-338080;AS-71070;CS-0324074;N'-(4-chlorobenzylidene)-4- methylbenzenesulfonohydrazide;(E)-N'-(4-Chlorobenzylidene)-4-methylbenzenesulfonohydrazide;N'-[(1E)-(4-Chlorophenyl)methylidene]-4-methylbenzene-1-sulfonohydrazide

Suppliers and Price of N'-(4-Chlorobenzylidene)-4-methylbenzenesulfonohydrazide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of N'-(4-Chlorobenzylidene)-4-methylbenzenesulfonohydrazide

Chemical Property:

XLogP3:3.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:4
Exact Mass:308.0386265
Heavy Atom Count:20
Complexity:417

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)S(=O)(=O)NN=CC2=CC=C(C=C2)Cl
Isomeric SMILES:CC1=CC=C(C=C1)S(=O)(=O)N/N=C/C2=CC=C(C=C2)Cl

Technology Process of N'-(4-Chlorobenzylidene)-4-methylbenzenesulfonohydrazide

There total 2 articles about N'-(4-Chlorobenzylidene)-4-methylbenzenesulfonohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 104-88-1
4-chlorobenzaldehyde

: 1576-35-8
toluene-4-sulfonic acid hydrazide

: 19350-69-7
4-chlorobenzaldehyde p-toluenesulfonylhydrazone

Guidance literature:: In neat (no solvent); at 20 ℃; for 0.0166667h; Solvent;
DOI:10.1002/open.201800206

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 19350-69-7
4-chlorobenzaldehyde p-toluenesulfonylhydrazone

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate / water; tetrahydrofuran / 0.5 h / 0 °C

2: methanol / Reflux

With hydrazine hydrate; In tetrahydrofuran; methanol; water;
DOI:10.1039/c5cc07833d

Reference yield: 96.0%

: 19350-69-7
4-chlorobenzaldehyde p-toluenesulfonylhydrazone

: 20025-49-4
4-chlorobenzyl 4'-methylphenyl sulfone

Guidance literature:: With iron(III)phthalocyanine chloride; potassium carbonate; In 1,4-dioxane; at 80 ℃; for 3h;
DOI:10.1016/j.tetlet.2016.04.044