N-[(E)-but-2-enyl]-N-(2,2-diethoxyethyl)-3-hydroxy-2-nitrobenzamide

Base Information

Chemical Name:N-[(E)-but-2-enyl]-N-(2,2-diethoxyethyl)-3-hydroxy-2-nitrobenzamide
CAS No.:94295-89-3
Molecular Formula:C₁₇H₂₄N₂O₆
Molecular Weight:352.387
Hs Code.:
NSC Number:343684
DSSTox Substance ID:DTXSID20422442
Wikidata:Q82234381

Synonyms:NSC343684;94295-89-3;DTXSID20422442;NSC-343684

Suppliers and Price of N-[(E)-but-2-enyl]-N-(2,2-diethoxyethyl)-3-hydroxy-2-nitrobenzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of N-[(E)-but-2-enyl]-N-(2,2-diethoxyethyl)-3-hydroxy-2-nitrobenzamide

Chemical Property:

Vapor Pressure:7.33E-11mmHg at 25°C
Boiling Point:506°C at 760 mmHg
Flash Point:259.8°C
Density:1.199g/cm³
XLogP3:2.9
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:9
Exact Mass:352.16343649
Heavy Atom Count:25
Complexity:445

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(CN(CC=CC)C(=O)C1=C(C(=CC=C1)O)[N+](=O)[O-])OCC
Isomeric SMILES:CCOC(CN(C/C=C/C)C(=O)C1=C(C(=CC=C1)O)[N+](=O)[O-])OCC

Technology Process of N-[(E)-but-2-enyl]-N-(2,2-diethoxyethyl)-3-hydroxy-2-nitrobenzamide

There total 3 articles about N-[(E)-but-2-enyl]-N-(2,2-diethoxyethyl)-3-hydroxy-2-nitrobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 602-00-6
3-hydroxy-2-nitrobenzoic acid

: 94295-89-3
N-((Z)-But-2-enyl)-N-(2,2-diethoxy-ethyl)-3-hydroxy-2-nitro-benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / dicyclohexylcarbodiimide / tetrahydrofuran / Ambient temperature

2: 1.) NaH / 1.) THF, RT, 1 h, 2.) THF, overnight

With sodium hydride; dicyclohexyl-carbodiimide; In tetrahydrofuran;
DOI:10.1021/jm00381a020

Reference yield:

: 645-36-3
2,2-diethoxy-ethanamine

: 94295-89-3
N-((Z)-But-2-enyl)-N-(2,2-diethoxy-ethyl)-3-hydroxy-2-nitro-benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / dicyclohexylcarbodiimide / tetrahydrofuran / Ambient temperature

2: 1.) NaH / 1.) THF, RT, 1 h, 2.) THF, overnight

With sodium hydride; dicyclohexyl-carbodiimide; In tetrahydrofuran;
DOI:10.1021/jm00381a020