N-(2-Thienylmethyl)-1-octanamine

Base Information

• Chemical Name: N-(2-Thienylmethyl)-1-octanamine
• CAS No.: 855379-69-0
• Molecular Formula: C₁₃H₂₃NS
• Molecular Weight: 225.398
• Mol file: 855379-69-0.mol

Synonyms:

Chemical Property of N-(2-Thienylmethyl)-1-octanamine

Chemical Property:

Purity/Quality:

98%min ^*data from raw suppliers

N-(2-Thienylmethyl)-1-octanamine ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi

MSDS Files:

Useful:

Technology Process of N-(2-Thienylmethyl)-1-octanamine

There total 3 articles about N-(2-Thienylmethyl)-1-octanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-Chloromethylthiophene (765-50-4) + n-Octylamine (111-86-4) → octyl-bis-[2]thienylmethyl-amine + octyl-[2]thienylmethyl-amine (855379-69-0)

Guidance literature:

With ethanol; sodium carbonate;

DOI:10.1021/ja01140a032

Reference yield:

1-octanamine,N-(2-thienylmethylene) → octyl-[2]thienylmethyl-amine (855379-69-0)

Guidance literature:

With sodium tetrahydroborate; at 20 ℃;

DOI:10.1111/j.1747-0285.2011.01231.x

Reference yield:

thiophene-2-carbaldehyde (98-03-3) + n-Octylamine (111-86-4) → octyl-[2]thienylmethyl-amine (855379-69-0)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium sulfate / methanol

2: sodium tetrahydroborate / 20 °C

With sodium tetrahydroborate; sodium sulfate; In methanol;

DOI:10.1111/j.1747-0285.2011.01231.x

upstream raw materials:

2-Chloromethylthiophene

n-Octylamine

thiophene-2-carbaldehyde

Refernces