Technology Process of C24H30ClN3O4
There total 7 articles about C24H30ClN3O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
N-ethyl-N,N-diisopropylamine;
In
N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 7 steps
1: N-ethyl-N,N-diisopropylamine / dichloromethane
2: N-iodo-succinimide; toluene-4-sulfonic acid / tetrahydrofuran; methanol
3: sodium hydride; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide; mineral oil
4: tri-n-butyl-tin hydride; 2,2'-azobis(isobutyronitrile) / toluene / 80 °C
5: hydrogenchloride / tetrahydrofuran; water; isopropyl alcohol
6: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 0 °C
7: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide
With
hydrogenchloride; N-iodo-succinimide; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; tetra-(n-butyl)ammonium iodide; sodium hydride; toluene-4-sulfonic acid; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; isopropyl alcohol; toluene; mineral oil;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: N-iodo-succinimide; toluene-4-sulfonic acid / tetrahydrofuran; methanol
2: sodium hydride; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide; mineral oil
3: tri-n-butyl-tin hydride; 2,2'-azobis(isobutyronitrile) / toluene / 80 °C
4: hydrogenchloride / tetrahydrofuran; water; isopropyl alcohol
5: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 0 °C
6: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide
With
hydrogenchloride; N-iodo-succinimide; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; tetra-(n-butyl)ammonium iodide; sodium hydride; toluene-4-sulfonic acid; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; methanol; water; N,N-dimethyl-formamide; isopropyl alcohol; toluene; mineral oil;