3-p-dimethylaminophenyl-3-phenylphthalide

Base Information

• Chemical Name: 3-p-dimethylaminophenyl-3-phenylphthalide
• CAS No.: 57302-23-5
• Molecular Formula: C₂₂H₁₉NO₂
• Molecular Weight: 329.398
• Mol file: 57302-23-5.mol

Synonyms:

Chemical Property of 3-p-dimethylaminophenyl-3-phenylphthalide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-p-dimethylaminophenyl-3-phenylphthalide

There total 2 articles about 3-p-dimethylaminophenyl-3-phenylphthalide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-p-dimethylaminophenyl-4-phenyl-3,4-dihydro-1(2H)-phthalazinone (76763-90-1) → 3-p-dimethylaminophenyl-3-phenylphthalide (57302-23-5) + 3-p-dimethylaminophenyl-3-phenyl-N-aminophthalimidine (76918-80-4)

Guidance literature:

With hydrogenchloride; for 2h; Heating;

DOI:10.1248/cpb.28.3561

Reference yield:

3-chloro-3-phenylphthalide (18852-53-4) + N,N-dimethyl-aniline (121-69-7,77733-26-7) → 3-p-dimethylaminophenyl-3-phenylphthalide (57302-23-5)

Guidance literature:

With aluminium trichloride; benzene;

Reference yield:

3-p-dimethylaminophenyl-3-phenylphthalide (57302-23-5) → 4-p-dimethylaminophenyl-4-phenyl-3,4-dihydro-1(2H)-phthalazinone (76763-90-1)

Guidance literature:

With hydrazine hydrate; In ethanol; at 70 ℃; for 72h; Rate constant;

DOI:10.1248/cpb.28.3561

upstream raw materials:

3-chloro-3-phenylphthalide

N,N-dimethyl-aniline

4-p-dimethylaminophenyl-4-phenyl-3,4-dihydro-1(2H)-phthalazinone

Downstream raw materials:

4-p-dimethylaminophenyl-4-phenyl-3,4-dihydro-1(2H)-phthalazinone