C₂₆H₁₉N

Base Information

• Chemical Name: C₂₆H₁₉N
• CAS No.: 936916-08-4
• Molecular Formula: C₂₆H₁₉N
• Molecular Weight: 345.444
• Mol file: 936916-08-4.mol

Synonyms:

Chemical Property of C₂₆H₁₉N

Chemical Property:

Purity/Quality:

97% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₆H₁₉N

There total 3 articles about C₂₆H₁₉N which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

9-(4'-chlorophenyl)phenanthrene (37842-69-6) + aniline (62-53-3) → C26H19N (936916-08-4)

Guidance literature:

With tri-tert-butyl phosphine; palladium diacetate; sodium t-butanolate; In o-xylene; at 60 - 130 ℃; for 15h; Inert atmosphere; Schlenk technique;

Reference yield:

9-phenanthrenylboronic acid (68572-87-2) → C26H19N (936916-08-4)

Guidance literature:

Multi-step reaction with 2 steps

1.1: sodium carbonate / tetrahydrofuran; water / 0.08 h / 20 °C / Inert atmosphere

1.2: 10 h / 65 °C

2.1: tri-tert-butyl phosphine; palladium diacetate; sodium t-butanolate / o-xylene / 15 h / 60 - 130 °C / Inert atmosphere; Schlenk technique

With tri-tert-butyl phosphine; palladium diacetate; sodium carbonate; sodium t-butanolate; In tetrahydrofuran; o-xylene; water;

Reference yield:

bromochlorobenzene (106-39-8) → C26H19N (936916-08-4)

Guidance literature:

Multi-step reaction with 2 steps

1.1: sodium carbonate / tetrahydrofuran; water / 0.08 h / 20 °C / Inert atmosphere

1.2: 10 h / 65 °C

2.1: tri-tert-butyl phosphine; palladium diacetate; sodium t-butanolate / o-xylene / 15 h / 60 - 130 °C / Inert atmosphere; Schlenk technique

With tri-tert-butyl phosphine; palladium diacetate; sodium carbonate; sodium t-butanolate; In tetrahydrofuran; o-xylene; water;

upstream raw materials:

bromochlorobenzene

9-phenanthrenylboronic acid

9-(4'-chlorophenyl)phenanthrene

aniline