Technology Process of 3,6-dihydro-9H-pyrazolo[4,3-f]quinazolin-9-one
There total 5 articles about 3,6-dihydro-9H-pyrazolo[4,3-f]quinazolin-9-one which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 89 percent / conc. HCl, hydroxylammoniumchloride, Na2SO4.10 H2O / H2O / 0.03 h / Heating
2: 63 percent / conc. H2SO4 / 0.17 h / 75 °C
3: 92 percent / 10percent NaOH, 10percent aq. H2O2 / 0.17 h / 100 °C
4: 64 percent / methanol; H2O; diethyl ether / 0.5 h / Ambient temperature
5: 78 percent / 1) 4 h, 140 deg C, 2) 2 h, 180 deg C
With
hydrogenchloride; sodium hydroxide; sulfuric acid; hydroxylamine hydrochloride; dihydrogen peroxide; sodium sulfate;
In
methanol; diethyl ether; water;
DOI:10.1002/cber.19811140506
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 92 percent / 10percent NaOH, 10percent aq. H2O2 / 0.17 h / 100 °C
2: 64 percent / methanol; H2O; diethyl ether / 0.5 h / Ambient temperature
3: 78 percent / 1) 4 h, 140 deg C, 2) 2 h, 180 deg C
With
sodium hydroxide; dihydrogen peroxide;
In
methanol; diethyl ether; water;
DOI:10.1002/cber.19811140506