PdBr(P(C₆H₅)3)2C₃NSBrCH₂OH

Base Information

• Chemical Name: PdBr(P(C₆H₅)3)2C₃NSBrCH₂OH
• CAS No.: 918164-48-4
• Molecular Formula: C₄₀H₃₃Br₂NOP₂PdS
• Molecular Weight: 903.95
• Mol file: 918164-48-4.mol

Synonyms:

Chemical Property of PdBr(P(C₆H₅)3)2C₃NSBrCH₂OH

Chemical Property:

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Technology Process of PdBr(P(C₆H₅)3)2C₃NSBrCH₂OH

There total 1 articles about PdBr(P(C₆H₅)3)2C₃NSBrCH₂OH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tetrakis(triphenylphosphine) palladium(0) (14221-01-3) + (2,4-dibromo-1,3-thiazol-5-yl)methanol (170232-68-5) → PdBr(P(C6H5)3)2C3NSBrCH2OH (918164-48-4)

Guidance literature:

In toluene; (Ar); stirring a mixt. of palladium complex and ligand in toluene overnight at room temp.; vac. evapn., trituration with Et2O, washing with Et2O, recrystn. (CHCl3/hexane or CH2Cl2/hexane); single crystal X-ray diffraction;

DOI:10.1039/b612235c

upstream raw materials:

tetrakis(triphenylphosphine) palladium⁽⁰⁾

(2,4-dibromo-1,3-thiazol-5-yl)methanol

Refernces