11-(4-chlorophenyl)-4-(3,5-dimethyl-1H-pyrazol-1-yl)-2-methyl-7,8,9,10-tetrahydropyrimido[4',5':4,5]thieno[2,3-b]quinoline

Base Information

Chemical Name:11-(4-chlorophenyl)-4-(3,5-dimethyl-1H-pyrazol-1-yl)-2-methyl-7,8,9,10-tetrahydropyrimido[4',5':4,5]thieno[2,3-b]quinoline
CAS No.:906375-90-4
Molecular Formula:C₂₅H₂₂ClN₅S
Molecular Weight:460.002
Hs Code.:
Mol file:906375-90-4.mol

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 11-(4-chlorophenyl)-4-(3,5-dimethyl-1H-pyrazol-1-yl)-2-methyl-7,8,9,10-tetrahydropyrimido[4',5':4,5]thieno[2,3-b]quinoline

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Technology Process of 11-(4-chlorophenyl)-4-(3,5-dimethyl-1H-pyrazol-1-yl)-2-methyl-7,8,9,10-tetrahydropyrimido[4',5':4,5]thieno[2,3-b]quinoline

There total 3 articles about 11-(4-chlorophenyl)-4-(3,5-dimethyl-1H-pyrazol-1-yl)-2-methyl-7,8,9,10-tetrahydropyrimido[4',5':4,5]thieno[2,3-b]quinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 906375-79-9
[5-(4-chloro-phenyl)-3-methyl-6,7,8,9-tetrahydro-11-thia-2,4,10-triaza-benzo[b]fluoren-1-yl]-hydrazine

: 123-54-6,81235-32-7
acetylacetone

: 906375-90-4
5-(4-chloro-phenyl)-1-(3,5-dimethyl-pyrazol-1-yl)-3-methyl-6,7,8,9-tetrahydro-11-thia-2,4,10-triaza-benzo[b]fluorene

Guidance literature:: for 4h; Heating;
DOI:10.1002/jccs.200500136

Reference yield:

: 906375-72-2
1-chloro-5-(4-chloro-phenyl)-3-methyl-6,7,8,9-tetrahydro-11-thia-2,4,10-triaza-benzo[b]fluorene

: 906375-90-4
5-(4-chloro-phenyl)-1-(3,5-dimethyl-pyrazol-1-yl)-3-methyl-6,7,8,9-tetrahydro-11-thia-2,4,10-triaza-benzo[b]fluorene

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / hydrazine hydrate / ethanol / 2 h / Heating

2: 82 percent / 4 h / Heating

With hydrazine hydrate; In ethanol;
DOI:10.1002/jccs.200500136

Reference yield:

: 136344-86-0
2-methyl-11-(p-chlorophenyl)-7,8,9,10-tetrahydroquinolino-<3',2':4,5>thieno<3,2-d>pyrimidin-4(3H)-one

: 906375-90-4
5-(4-chloro-phenyl)-1-(3,5-dimethyl-pyrazol-1-yl)-3-methyl-6,7,8,9-tetrahydro-11-thia-2,4,10-triaza-benzo[b]fluorene

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / phosphorus oxychloride / 4 h / Heating

2: 85 percent / hydrazine hydrate / ethanol / 2 h / Heating

3: 82 percent / 4 h / Heating

With hydrazine hydrate; trichlorophosphate; In ethanol;
DOI:10.1002/jccs.200500136