1,1-DIMETHYL-3,4-DIPHENYL-2-TRIMETHYLSILANYL-5-TRIPHENYLSILANYL-1H-SILOLE

Base Information

• Chemical Name: 1,1-DIMETHYL-3,4-DIPHENYL-2-TRIMETHYLSILANYL-5-TRIPHENYLSILANYL-1H-SILOLE
• CAS No.: 934563-23-2
• Molecular Formula: C₃₉H₄₀Si₃
• Molecular Weight: 593.003
• Mol file: 934563-23-2.mol

Synonyms:

Chemical Property of 1,1-DIMETHYL-3,4-DIPHENYL-2-TRIMETHYLSILANYL-5-TRIPHENYLSILANYL-1H-SILOLE

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,1-DIMETHYL-3,4-DIPHENYL-2-TRIMETHYLSILANYL-5-TRIPHENYLSILANYL-1H-SILOLE

There total 1 articles about 1,1-DIMETHYL-3,4-DIPHENYL-2-TRIMETHYLSILANYL-5-TRIPHENYLSILANYL-1H-SILOLE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

(1Z,3Z)-1,4-bis(trimethylsilyl)-2,3-diphenyl-1,4-diiodo-1,3-butadiene + Triphenylsilyl chloride (76-86-8) → C39H40Si3 (934563-23-2)

Guidance literature:

(1Z,3Z)-1,4-bis(trimethylsilyl)-2,3-diphenyl-1,4-diiodo-1,3-butadiene; With tert.-butyl lithium; In diethyl ether; pentane; at -78 ℃; for 1h;

With N,N,N,N,N,N-hexamethylphosphoric triamide; In diethyl ether; pentane; for 1h; Heating;

Triphenylsilyl chloride; In diethyl ether; pentane; at 20 ℃; for 1h; Further stages.;

DOI:10.1021/ja070404s

upstream raw materials:

Triphenylsilyl chloride