C₁₀H₁₈O₂

Base Information

Chemical Name:C₁₀H₁₈O₂
CAS No.:1330119-07-7
Molecular Formula:C₁₀H₁₈O₂
Molecular Weight:170.252
Hs Code.:

C<sub>10</sub>H<sub>18</sub>O<sub>2</sub>

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₀H₁₈O₂

Chemical Property:

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Technology Process of C₁₀H₁₈O₂

There total 6 articles about C₁₀H₁₈O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C₉H₁₆O₃: C₉H₁₆O₃

: 1779-49-3
Methyltriphenylphosphonium bromide

: 1330119-07-7
C₁₀H₁₈O₂

Guidance literature:: Methyltriphenylphosphonium bromide; With potassium tert-butylate; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;

C₉H₁₆O₃; In tetrahydrofuran; at 0 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ml1002184

Reference yield:

: C₁₄H₂₆O₄

: 1330119-07-7
C₁₀H₁₈O₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: methyllithium / diethyl ether / 0.5 h / 0 °C / Inert atmosphere

2.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C

2.2: -78 - 20 °C

3.1: potassium tert-butylate / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

3.2: 2 h / 0 °C / Inert atmosphere

With oxalyl dichloride; potassium tert-butylate; methyllithium; dimethyl sulfoxide; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1021/ml1002184

Reference yield:

C₉H₁₈O₃: C₉H₁₈O₃

: 1330119-07-7
C₁₀H₁₈O₂

Guidance literature:: Multi-step reaction with 2 steps

1.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C

1.2: -78 - 20 °C

2.1: potassium tert-butylate / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

2.2: 2 h / 0 °C / Inert atmosphere

With oxalyl dichloride; potassium tert-butylate; dimethyl sulfoxide; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ml1002184