Carbamic acid, (1-formyl-3-phenylpropyl)-, 1,1-dimethylethyl ester

Base Information

• Chemical Name: Carbamic acid, (1-formyl-3-phenylpropyl)-, 1,1-dimethylethyl ester
• CAS No.: 140196-39-0
• Molecular Formula: C15H21NO3
• Molecular Weight: 263.33200
• Mol file: 140196-39-0.mol

Synonyms:1,1-Dimethylethyl 1-formyl-3-phenylpropylcarbamate;Carbamic acid,(1-formyl-3-phenylpropyl)-,1,1-dimethylethyl ester;

Chemical Property of Carbamic acid, (1-formyl-3-phenylpropyl)-, 1,1-dimethylethyl ester

Chemical Property:

• PSA: 58.89000
• LogP: 2.91580

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Carbamic acid, (1-formyl-3-phenylpropyl)-, 1,1-dimethylethyl ester

There total 2 articles about Carbamic acid, (1-formyl-3-phenylpropyl)-, 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-methoxy-N-methyl-2-(N-(tert-butoxycarbonyl)amino)-4-phenylbutanamide (294871-39-9) → 1,1-Dimethylethyl 1-formyl-3-phenylpropylcarbamate (140196-39-0)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether; at 0 ℃; for 2h; Inert atmosphere;

DOI:10.1039/c7md00592j

Reference yield:

→ 1,1-Dimethylethyl 1-formyl-3-phenylpropylcarbamate (140196-39-0)

Guidance literature:

Reference yield: 70.0%

(S)-(2-(2-((1-(tert-butoxycarbonyl)-1H-indol-3-yl)methyl)-3-methoxy-5-oxo-2,5-dihydro-1H-pyrrol-1-yl)-2-oxoethyl )triphenylphosphonium chloride + 1,1-Dimethylethyl 1-formyl-3-phenylpropylcarbamate (140196-39-0) → C36H43N3O7

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 35 ℃; for 12h;

DOI:10.1021/acs.jmedchem.1c01494

upstream raw materials:

N-methoxy-N-methyl-2-(N-(tert-butoxycarbonyl)amino)-4-phenylbutanamide

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