4-(1-bromo-2-methylpropan-2-yl)-3,6-dichloropyridazine

Base Information

Chemical Name:4-(1-bromo-2-methylpropan-2-yl)-3,6-dichloropyridazine
CAS No.:108287-80-5
Molecular Formula:C₈H₉BrCl₂N₂
Molecular Weight:283.983
Hs Code.:
Mol file:108287-80-5.mol

Synonyms:

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Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-(1-bromo-2-methylpropan-2-yl)-3,6-dichloropyridazine

Chemical Property:

Vapor Pressure:6.78E-05mmHg at 25°C
Boiling Point:354.6°C at 760 mmHg
Flash Point:168.2°C
Density:1.58g/cm³

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 4-(1-bromo-2-methylpropan-2-yl)-3,6-dichloropyridazine

There total 3 articles about 4-(1-bromo-2-methylpropan-2-yl)-3,6-dichloropyridazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 108288-03-5
3,6-dichloro-β,β-dimethyl-4-pyridazineethanol 4-methylbenzenesulfonate ester

: 108287-80-5
3,6-dichloro-4-(2-bromo-1,1-dimethylethyl)pyridazine

Guidance literature:: With lithium bromide; In dimethyl sulfoxide; at 110 ℃; for 2h;
DOI:10.1021/jo00259a018

Reference yield:

: 108288-02-4
3,6-dichloro-β,β-dimethyl-4-pyridazineethanol

: 108287-80-5
3,6-dichloro-4-(2-bromo-1,1-dimethylethyl)pyridazine

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / pyridine / 17 h / 25 °C

2: 91 percent / LiBr / dimethylsulfoxide / 2 h / 110 °C

With pyridine; lithium bromide; In dimethyl sulfoxide;
DOI:10.1021/jo00259a018