3-BROMO-2-FORMYLPHENYLBORONIC ACID

Base Information

• Chemical Name: 3-BROMO-2-FORMYLPHENYLBORONIC ACID
• CAS No.: 928048-12-8
• Molecular Formula: C₇H₆BBrO₃
• Molecular Weight: 228.838
• Mol file: 928048-12-8.mol

Synonyms:

Chemical Property of 3-BROMO-2-FORMYLPHENYLBORONIC ACID

Chemical Property:

• Boiling Point: 402.5±55.0 °C(Predicted)
• PKA: 7.21±0.53(Predicted)
• Density: 1.71±0.1 g/cm3(Predicted)
• Storage Temp.: 2-8°C

Purity/Quality:

HPLC≥98% ^*data from raw suppliers

(3-Bromo-2-formylphenyl)boronicAcid ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-BROMO-2-FORMYLPHENYLBORONIC ACID

There total 3 articles about 3-BROMO-2-FORMYLPHENYLBORONIC ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

1,3-dibromo-2-(dimethoxymethyl)benzene (928048-21-9) → (3-bromo-2-formylphenyl)boronic acid (928048-12-8)

Guidance literature:

1,3-dibromo-2-(dimethoxymethyl)benzene; With n-butyllithium; In diethyl ether; at -78 ℃; for 0.25h;

With triethyl borate; In diethyl ether; at -78 - -50 ℃; for 0.5h; Further stages.;

DOI:10.1039/b611195e

Reference yield:

2,6-dibromobenzaldehyde (67713-23-9) → (3-bromo-2-formylphenyl)boronic acid (928048-12-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 98 percent / H₂SO₄ / methanol / 1 h / Heating

With sulfuric acid; In methanol;

DOI:10.1039/b611195e

Reference yield:

1,3-dibromo-2-(dimethoxymethyl)benzene (928048-21-9) → 3-iodo-2-formylphenylboronic acid (928048-13-9) + (3-bromo-2-formylphenyl)boronic acid (928048-12-8)

Guidance literature:

Multistep reaction.;

DOI:10.1039/b611195e

upstream raw materials:

1,3-dibromo-2-(dimethoxymethyl)benzene

2,6-dibromobenzaldehyde

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 928048-12-8 3-BROMO-2-FORMYLPHENYLBORONIC ACID

Send

Send

Metric Ton KG G Pound L ML

Send

Send