4-Methoxynaphthalen-1-amine hydrochloride

Base Information

• Chemical Name: 4-Methoxynaphthalen-1-amine hydrochloride
• CAS No.: 92599-05-8
• Molecular Formula: C₁₁H₁₁NO*ClH
• Molecular Weight: 209.675
• ChEMBL ID: CHEMBL4175261
• DSSTox Substance ID: DTXSID80596214
• Mol file: 92599-05-8.mol

Synonyms:4-Methoxynaphthalen-1-amine hydrochloride;92599-05-8;1-Amino-4-methoxynaphthalen HCl;4-methoxynaphthalen-1-amine;hydrochloride;1-Amino-4-methoxynaphthalen hydrochloride;1-Naphthalenamine, 4-methoxy-, hydrochloride;1-amino-4-methoxynaphthalene hydrochloride;4-Methoxynaphthalen-1-aminehydrochloride;SCHEMBL6155452;CHEMBL4175261;4-Methoxynaphthalen-1-amine HCl;DTXSID80596214;MFCD16877105;AKOS015999240;BS-33179;CS-0150361;D95116;EN300-314264;A860038;4-Methoxynaphthalen-1-amine--hydrogen chloride (1/1);F2146-0572;Z2681942354

Chemical Property of 4-Methoxynaphthalen-1-amine hydrochloride

Chemical Property:

• Melting Point: 278-279 °C (decomp)
• Storage Temp.: Sealed in dry,Room Temperature
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 1
• Exact Mass: 209.0607417
• Heavy Atom Count: 14
• Complexity: 172

Purity/Quality:

97% ^*data from raw suppliers

1-Amino-4-methoxynaphthalenhydrochloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: COC1=CC=C(C2=CC=CC=C21)N.Cl
• Uses: 1-Amino-4-methoxynaphthalen HCl

Technology Process of 4-Methoxynaphthalen-1-amine hydrochloride

There total 3 articles about 4-Methoxynaphthalen-1-amine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

1-methoxy-4-nitronaphthalene (4900-63-4) → 1-amino-4-methoxynapthalene hydrochloride (92599-05-8)

Guidance literature:

1-methoxy-4-nitronaphthalene; With hydrazine hydrate; In methanol; for 2h; Reflux;

With hydrogenchloride; In 1,4-dioxane; diethyl ether;

DOI:10.1016/j.ejmech.2017.05.015

Reference yield:

1-Methoxynaphthalene (2216-69-5) → 1-amino-4-methoxynapthalene hydrochloride (92599-05-8)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium nitrate; benzyltriphenylphosphonium peroxodisulfate / acetonitrile / 5 h / Reflux

2: hydrazine hydrate / methanol / 2 h / Reflux

With sodium nitrate; hydrazine hydrate; benzyltriphenylphosphonium peroxodisulfate; In methanol; acetonitrile;

DOI:10.1016/j.ejmech.2017.05.015

Reference yield:

→ 1-amino-4-methoxynapthalene hydrochloride (92599-05-8)

Guidance literature:

upstream raw materials:

1-methoxy-4-nitronaphthalene

1-Methoxynaphthalene

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