2-carboxyphenyl beta-D-glucopyranosiduronic acid

Base Information

Chemical Name:2-carboxyphenyl beta-D-glucopyranosiduronic acid
CAS No.:7696-34-6
Molecular Formula:C₁₃H₁₄O₉
Molecular Weight:314.249
Hs Code.:

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Chemical Property of 2-carboxyphenyl beta-D-glucopyranosiduronic acid

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Technology Process of 2-carboxyphenyl beta-D-glucopyranosiduronic acid

There total 6 articles about 2-carboxyphenyl beta-D-glucopyranosiduronic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 138-52-3
D-(-)-salicin

: 7695-70-7,31566-22-0,7696-34-6,96750-93-5
Salicylic acid phenol glucuronide

Guidance literature:: With 2,2,6,6-tetramethyl-piperidine-N-oxyl; Carbonate buffer; at 20 ℃; Yield given; electrochemical reaction: platinum foil anode and a graphite cathode, saturated calomel electrode as reference electrode (Hg/Hg₂Cl₂/saturated KCl in H₂O, +0.20 V vs. SCE), electrolysis at a potential of 0.53 V vs. SCE, charge consumption of 11.2 F/mol;
DOI:10.1055/s-1999-3464

Reference yield:

: 101231-54-3
O²,O³,O⁴-triacetyl-O¹-(2-methoxycarbonyl-phenyl)-β-D-glucopyranuronic acid methyl ester

: 7695-70-7,31566-22-0,7696-34-6,96750-93-5
Salicylic acid phenol glucuronide

Guidance literature:: With barium dihydroxide; water;
DOI:10.1021/jo01111a603

Reference yield:

: 21085-72-3
1-bromo-2,3,4-tri-O-acetyl-α-D-glucuronic acid methyl ester

: 7695-70-7,31566-22-0,7696-34-6,96750-93-5
Salicylic acid phenol glucuronide

Guidance literature:: Multi-step reaction with 2 steps

1: silver oxide; isoquinoline

2: barium hydroxide; water

With isoquinoline; barium dihydroxide; water; silver(l) oxide;
DOI:10.1021/jo01111a603