Trichothec-9-ene-4,15-diol, 12,13-epoxy-, 15-(3-methyl-2,4-pentadienoate), (4beta,15(Z))-

Base Information

Chemical Name:Trichothec-9-ene-4,15-diol, 12,13-epoxy-, 15-(3-methyl-2,4-pentadienoate), (4beta,15(Z))-
CAS No.:89015-96-3
Molecular Formula:C₂₁H₂₈O₅
Molecular Weight:360.45
Hs Code.:

Synonyms:89015-96-3;Trichothec-9-ene-4,15-diol, 12,13-epoxy-, 15-(3-methyl-2,4-pentadienoate), (4beta,15(Z))-

Suppliers and Price of Trichothec-9-ene-4,15-diol, 12,13-epoxy-, 15-(3-methyl-2,4-pentadienoate), (4beta,15(Z))-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Trichothec-9-ene-4,15-diol, 12,13-epoxy-, 15-(3-methyl-2,4-pentadienoate), (4beta,15(Z))-

Chemical Property:

Vapor Pressure:5.49E-12mmHg at 25°C
XLogP3:2.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:5
Exact Mass:360.19367399
Heavy Atom Count:26
Complexity:709

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=CC2C(CC1)(C3(C(CC(C34CO4)O2)O)C)COC(=O)C=C(C)C=C
Isomeric SMILES:CC1=CC2C(CC1)(C3(C(CC(C34CO4)O2)O)C)COC(=O)/C=C(/C)\C=C

Technology Process of Trichothec-9-ene-4,15-diol, 12,13-epoxy-, 15-(3-methyl-2,4-pentadienoate), (4beta,15(Z))-

There total 3 articles about Trichothec-9-ene-4,15-diol, 12,13-epoxy-, 15-(3-methyl-2,4-pentadienoate), (4beta,15(Z))- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 19.0%

: 88968-94-9
(E)-5-[2-(Dimethoxy-phosphoryl)-acetoxy]-3-methyl-pent-2-enoic acid

: 2198-92-7
Verrucarol

: 84303-86-6,89015-96-3,89103-57-1
C₂₁H₂₈O₅

: 84303-87-7
C₁₉H₂₉O₈P

: 84303-84-4,84303-85-5
Trichothecene monoester

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; Title compound not separated from byproducts;
DOI:10.1021/jo00153a035

Reference yield:

: 88969-03-3
(E)-5-[2-(Dimethoxy-phosphoryl)-acetoxy]-3-methyl-pent-2-enoic acid 2,2,2-trichloro-ethyl ester

: 84303-86-6,89015-96-3,89103-57-1
C₂₁H₂₈O₅

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / Zn, KH₂PO₄ / tetrahydrofuran

2: 19 percent / DCC, DMAP / CH₂Cl₂

With dmap; potassium dihydrogenphosphate; dicyclohexyl-carbodiimide; zinc; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo00153a035

Reference yield:

: 88968-95-0
2,2,2-Trichloroethyl 5-Hydroxy-3-methyl-2(E)-pentenoate

: 84303-86-6,89015-96-3,89103-57-1
C₂₁H₂₈O₅

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / Trifluoroacetic anhydride, Pyridine / CH₂Cl₂

2: 76 percent / Zn, KH₂PO₄ / tetrahydrofuran

3: 19 percent / DCC, DMAP / CH₂Cl₂

With pyridine; dmap; potassium dihydrogenphosphate; dicyclohexyl-carbodiimide; trifluoroacetic anhydride; zinc; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo00153a035