Technology Process of C16H16FN3O2S2
There total 8 articles about C16H16FN3O2S2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C13H12FN3O2S2;
With
potassium carbonate;
In
acetone;
at 20 ℃;
for 0.166667h;
3-haloprop-1-ene;
In
acetone;
for 0.5h;
DOI:10.1021/jf9026298
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: sodium hydroxide / dichloromethane; water / 0.5 h / Cooling with ice
2.1: dichloromethane / 20 °C
3.1: triethylamine / toluene / 20 °C / Inert atmosphere; Reflux
4.1: sulfuric acid; nitric acid / Cooling with ice
5.1: iron; ammonium chloride / ethanol; water / Reflux
6.1: N,N-dimethyl-formamide / 3 h / 120 °C
7.1: potassium carbonate / acetone / 0.17 h / 20 °C
7.2: 0.5 h
With
sulfuric acid; nitric acid; iron; potassium carbonate; ammonium chloride; triethylamine; sodium hydroxide;
In
ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetone; toluene;
DOI:10.1021/jf9026298
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sulfuric acid; nitric acid / Cooling with ice
2.1: iron; ammonium chloride / ethanol; water / Reflux
3.1: N,N-dimethyl-formamide / 3 h / 120 °C
4.1: potassium carbonate / acetone / 0.17 h / 20 °C
4.2: 0.5 h
With
sulfuric acid; nitric acid; iron; potassium carbonate; ammonium chloride;
In
ethanol; water; N,N-dimethyl-formamide; acetone;
DOI:10.1021/jf9026298
