R-(-)-(1-(2)H)agmatine sulfate

Base Information

• Chemical Name: R-(-)-(1-(2)H)agmatine sulfate
• CAS No.: 83544-67-6
• Molecular Formula: C₅H₁₄N₄*H₂O₄S
• Molecular Weight: 229.264
• Mol file: 83544-67-6.mol

Synonyms:

Chemical Property of R-(-)-(1-(2)H)agmatine sulfate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of R-(-)-(1-(2)H)agmatine sulfate

There total 4 articles about R-(-)-(1-(2)H)agmatine sulfate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

L-arginine hydrochloride (1119-34-2) → R-(-)-(1-(2)H)agmatine sulfate (83544-67-6)

Guidance literature:

L-arginine decarboxylase; In water-d2; at 36 ℃; for 40h;

DOI:10.1016/S0040-4020(01)88666-X

Reference yield:

N-acetyl-L-arginine (155-84-0) → R-(-)-(1-(2)H)agmatine sulfate (83544-67-6)

Guidance literature:

Multi-step reaction with 3 steps

1: 1) deuterium oxide; 2) acetic anhydride; 3) deuterium oxide / 2) perdeuterio acetic acid, reflux, 2 h; 3) reflux, 30 min

2: hog kidney acylase I

3: 100 mg / 40 h / 36 °C / enzymic decarboxylation with L-arginine decarboxylase

With water-d2; acetic anhydride;

DOI:10.1139/v82-404

Reference yield:

L-(2-(2)H)arginine monohydrochloride (83544-61-0) → R-(-)-(1-(2)H)agmatine sulfate (83544-67-6)

Guidance literature:

at 36 ℃; for 40h; enzymic decarboxylation with L-arginine decarboxylase;

DOI:10.1139/v82-404

upstream raw materials:

L-arginine hydrochloride

L-(2-⁽²⁾H)arginine monohydrochloride

N-acetyl-L-arginine

α-N-acetyl-DL-(2-(2)H)arginine