11-Nor-Δ9-Tetrahydro Cannabinol-9-carboxylic-d5 Acid

Base Information

Chemical Name:11-Nor-Δ9-Tetrahydro Cannabinol-9-carboxylic-d5 Acid
CAS No.:949596-03-6
Molecular Formula:C₁₉H₂₄O₄
Molecular Weight:321.357
Hs Code.:
Mol file:949596-03-6.mol

Synonyms:

Suppliers and Price of 11-Nor-Δ9-Tetrahydro Cannabinol-9-carboxylic-d5 Acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 11-Nor-Δ9-Tetrahydro Cannabinol-9-carboxylic-d5 Acid

Chemical Property:

Purity/Quality:: >98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Uses Isotope labelled 11-Nor-Δ9-Tetrahydro Cannabinol-9-carboxylic Acid

Technology Process of 11-Nor-Δ9-Tetrahydro Cannabinol-9-carboxylic-d5 Acid

There total 2 articles about 11-Nor-Δ9-Tetrahydro Cannabinol-9-carboxylic-d5 Acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 949595-97-5
C₃₃H₄₃⁽²⁾H₅N₂SO₄

: 124-38-9,18923-20-1
carbon dioxide

: 949596-03-6
(6aR,10aR)-6a,7,8,10a-tetrahydro-1-hydroxy-6,6-dimethyl-3-(2',2',3',3',3'-²H₅-propyl)-6H-dibenzo[b,d]pyran-9-carboxylic acid

: C₁₉H₁₉⁽²⁾H₅O₄

Guidance literature:: C₃₃H₄₃⁽²⁾H₅N₂SO₄; With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In hexane; at -78 - 0 ℃; for 1.5h;

carbon dioxide; In hexane; at 0 ℃; for 0.166667h; Further stages.;
DOI:10.1016/j.tet.2007.06.006

Reference yield:

: 949595-92-0
(6aR,10aR)-6,6a,7,8,10,10a-hexahydro-1-hydroxy-6,6-dimethyl-3-(2',2',3',3',3'-²H₅-propyl)-9H-dibenzo[b,d]pyran-9-one

: 949596-03-6
(6aR,10aR)-6a,7,8,10a-tetrahydro-1-hydroxy-6,6-dimethyl-3-(2',2',3',3',3'-²H₅-propyl)-6H-dibenzo[b,d]pyran-9-carboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: benzene / 0.17 h / 40 - 42 °C

2.1: n-butyllithium; N,N,N',N'-tetramethylethylenediamine / hexane / 1.5 h / -78 - 0 °C

2.2: 270 mg / hexane / 0.17 h / 0 °C

With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In hexane; benzene; 2.1: Shapiro reaction;
DOI:10.1016/j.tet.2007.06.006